SASE3 instruments - status and plans - soon - European XFEL
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SASE3 instruments – status and plans
European XFEL Users’ Meeting 2018
Serguei Molodtsov
European XFEL, Scientific Director
Hamburg, January 24, 2018
+ soon….
SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 2
Overview
Undulator systems
Optics and diagnostics
Experimental hutches
Optical lasers
Detectors
Sample environment
Scientific instruments
SASE2 SASE1 SASE3
SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 3
SASE System without With enclosure All gaps closed to 10 mm
• Hardware installed & aligned • All gaps can be closed to 10 mm
• Control system & remote controls operational • System is fully operational
• Air conditioning commissioned & operational • Final system tests were done
SASE3 undulator is fully operational since the end of March 2017
SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 4
Implementation of circular polarization in 2020, cooperation with SwissFEL
Boundary condition of the design considered was minimum invasiveness to the SwissFEL/PSI
undulator layout with the main goal to decrease implementation costs.
Afterburner sections length (2 m) and the precise mechanics were selected to be the same in
both cases for the European XFEL afterburners and the undulator of SwissFEL/PSI.
Solution presented allows using intersections, phase shifters, and quadrupole movers already
used at the European XFEL.
SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 5
Optics & vacuum components installation summary SASE3
All components are delivered and installed.
Racks & cables: Most essential cables for first commissioning are in place.
Vacuum system is complete and closed.
Controls: Vacuum complete and in operation. Motion control under local testing and Karabo
projects are being set up.
Optics: Two offset mirrors and optics for soft-X-ray monochromator (2 pre-mirrors, 1 short
grating, 1 long grating blank) are installed.
First lasing is expected in the beginning of February. Commissioning of beam transport in
XTD10 will start on February 14.
SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 6
Current view of SASE3, XTD10 tunnel Vacuum Control System (PLC/Karabo)
Offset
Mirrors
SASE3 main vacuum control panel
SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 7
Diagnostics installation summary SASE3
Systems:
FILT, IMGTR, KMONO, IMGSR, XGM, DP (PES related differential pumping), PES,
IMGFEL, MCP-detector, IMGPIII, IMGPII90, IMGPII45, 2 x IMGES, 3 x IMGPI
Mechanics / UHV chambers
All supports installed and surveyed
All vacuum chambers installed and connected to beamline vacuum
Gas supply system installed, tested, flushed; operational for XGM
All electronics and cabling installation completed (except PES)
Technical commissioning without beam
Completed for XGM, DP, Imagers. Ongoing for MCP, KMONO
not started for PES (on locally controlled vacuum operation)
SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 8
MCP detector
SASE3 photon diagnostics
K-monochromator
X-ray gas monitor (XGM)
here is shown the fully assembled version of XTD2
Photoemission spectrometer in XTD10
SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 9
SASE3 photon diagnostics: imagers
Type III FEL imager
pop-in monitor
SR imager Two Exit Slit imagers
Type II-90 pop-in monitor Type II-45 pop-in 3 pop-ins Type I
SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 10
SASE3: Status of the civil construction
Laser hutches: Done.
Experimental hutches: Done.
Control and rack hutches: Done.SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 11
SASE3: Status of the technical infrastructure installation
AC / Cooling: AC devices are in place
and are being prepared for
commissioning. Will provide clean air
from middle of March 2018.
Electrical inst.: Cable trays done,
power cabinets in place, being hooked
up. Should be ready by mid of March.
Sanitary: Working, not critical.
Gases: Preparing for final acceptance
tests.
Fire safety: 95% done.SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 12
SASE3: Status of the cabling / PLC planning
IT cabling: Done, final acceptance test
planned for the middle of Feb. IT
connectivity available mid of March.
PLC modules production: ca. 80%
produced & tested. Remaining modules
produced until March.
Phase II cabling (motors, sensors…):
All cabling done in April 2018.
Scope of planning & work: 160+ PLC
modules + 3200+ associated cables (not
counting power or IT)!
Start of electronics and cabling
commissioning: April 2018SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 13
SASE3: 2018 schedule
First Lasing in February 2018, beam
brought up to the end of photon tunnels
Major infrastructure works will finish in
March/April
Day 1 instrument installation starting in full
swing in March/April
Commissioning of instrument controls &
electronics without beam in May/June/July
Instrument commissioning with beam in
August/September
Very first trial experiments in October
Potential first scheduled users in middle of
NovemberSASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 14
PP-laser installation schedule
n General PP-laser installation schedule:
Task 1: Laser tables and infrastructure in PP and ILH-hutches
Task 2: Components + commissioning in PP and ILH-hutches
Task 3: Beam to experiment
n Challenges:
Ø Parallel installation at SASE 2 and 3
n SASE-specific schedules:
Ø Simultaneous operation at SASE 1
Year Jul 2016 Dec Jan 2017 Dec Jan 2018 Dec Jan 2019 Dec
SASE1
SASE3
SASE2SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 15
DSSC MiniSDD1 Mpix Detector Processed DEPFET Wafer
Vacuum Cooling
Vessel Block
Electronics/Power Courtesy DSSC Collaboration
Provided by pnSensor GmbH
Measured DEPFET Characteristics
Project started one year later
Production of detector components almost completed
Front-end electronics produced and successfully tested
Collaboration is focused on integrating, calibrating and commissioning of the
first full size 1 Mpix camera based on MiniSDD sensors, to be ready in Q3 2018
Full specs DEPFET based camera will follow in January 2020
Provided by pnSensor GmbHSASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 16
pnCCD FastCCD
FastCCD
Detector arrived at XFEL
Beamline integration at SCS
is in progress
Calibration is in progress
Ready for installation at
experiment May 2018
pnCCD
Energy Range Energy Range
Detector for soft- and hard X-
0.03 – 25 keV 0.25 – 6 keV
ray imaging experiments.
Pixel Size 75 x 75 μm2 Pixel Size 30 x 30 μm2
Procurement and testing of
1024 x 1024 Pixels2 1920 x 960 Pixels2
first components started.
Dynamic Range Dynamic Range
Detector available in autumn Approx. 350 ph@1 keV
6000 ph@1.keV
2018.
Frame Rate Frame Rate
Primary experiments up to 150 Hz up to 200 Hz
SQS and SCS Noise Noise
6 e- at high gain 25 e- at high gainSASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 17
Fast solid sample scanner
Storage and DC electromagnet environment
Load Lock System
Fast Solid Sample
Scanner
Transfer Arm
Gate Valve
Linear motor
Turbo Pump
100 mm18
SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 18
Final Layout of SQS Scientific Instrument Timing Beam
Diagnostics Dump
AQS
Atomic-like Quantum Systems NQS
Targets: atoms & molecules
Detection: electrons, ions, photons
AQS
KB Optics
Bendable mirrors
3 interaction points
FEL Diagnostics
NQS
Nano-size Quantum Systems
Targets: Cluster, Nano-particles, bio-molecules
Detection: electrons, ions, photons
SQS-REMI
Reaction Microscope
Targets: molecules
Detection: electrons, ions
Angle- and energy-resolved
electron and ion spectra
in coincidence19
SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 19
Atomic-like Quantum
Layout of SQS for Systems AQS Beam
atoms & molecules Dump
DAY-1 Operation Detection: electrons, ions,
photons
KB Optics: - interim solution
- non bendable KB Optics
à 1 interaction point NQS
à exchange of chambers
FEL Diagnostics
Nano-size Quantum
REMI Systems
Cluster, Nano-particles, bio-
molecules
Reaction Microscope Detection: electrons, ions,
Molecules, Detection: electrons, ions photons
Angle- and energy-resolved
electron and ion spectra in
coincidence20
SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 20
Vacuum vessel VMI
AQS assembly & test (< 10-10 mbar) E ≤ 1 keV, E/DE=100
OK✔
testing
eTOF: E/DE > 10 000
Precision alignment base (1 µm)
OK✔
AQS: Atomic-like Quantum Systems
6 x eTOFs High energy resolution
Non-dipole studies
1 x VMI Angular distribution
e / ion – coincidences
1 x MBES e / e – coincidences OK✔
1 1D Imaging XUV spectrometerSASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 21
SQS Installation schedule
2017 2018 2019
Q3 Q4 Q1 Q2 Q3 Q4 Q1 Q2
Assembly & Testing Installation Operation with BEAM
Diagnostics
SQS Early User Workshop
KB focussing system
12-13 February 2018
AQS chamber Schenefeld campus User Operation
NQS chamber
REMI chamber
Hutch handover (Mar ‘18) First beam in hutch
Infrastructure ready (May ‘18) (> Aug ‘18)
Hutch operational (Aug ‘18)SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 22
Spectroscopy and Coherent scattering (SCS) scientific instrument
Configuration at start of operation
Alignment Laser
X-ray pulse intensity monitor
Visible / IR laser delivery
Fast CCD module
DSSC module
X-ray refocusing optics
KB mirror benders
1 - 500µm spot diam.
FFT experiment station
XAS, SAXS, CDI
Fixed Targets
Fast sample scanner
DC magnetic field Transmission MonitorSASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 23
SCS instrument timeline and status
May 2017 - Instrument components stored in
experiment hall, local testing of FFT station and
pre-installations
Dec. 2017 - KB mirror system stored at FMB
Oxford
Jan 2018 – superpolished JTEC mirrors delivered,
inspection in metrology labs.
March 2018 - Start of sensitive component
installation
May/June 2018 Day-one components installed and
FastCCD integrated. Controls and DAQ to continue
August 2018 commissioning startSASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 24
SCS 2nd baseline instrument (2019): Time-resolved spectroscopy:
XRD experiment station X-ray absorption spectroscopy (XAS)
UHV, 10-9
mbar
Sample-transfer port Resonant inelastic x-ray scattering (RIXS)
in-vacuum diffractometer, 2
degrees of motion Reflectivity / X-ray resonant diffraction (XRD)
sample stage: 6 degrees of
motion Pump
cryogenic conditions
THz laser incoupling Detector
Probe Signal
Rotable port:
SCS Early User Workshop
Sample
in-vacuum rotation for 21-22 February 2018
scattering angle range
60 deg – 150 deg Schenefeld campus
Magnetization dynamics in correlated materials:
Magnetic order: Magnetic correlations:
M.P.M. Dean et al., Nat. mat. 15, 601 (2016)SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 25
SCS and hRIXS user consortium: hRIXS working group (on behalf of the consortium):
Heisenberg RIXS setup
hRIXS spectrometer G. Ghiringhelli, A. Scherz, J. Schlappa, J.T. Delitz, T.
sample chamber
Laarmann, S. Techert, S. Huotari, F. Senf, A. Pietzsch,
(exchangable) S. Neppl and A. Föhlisch
Spectrometer:
Tender awarded (Bestec GmbH); delivery April 2019
Detector:
Multi-hit compatible delay-line anode contributed by
Finnish partner consortium
High-quality floorSASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 26
Chemistry Endstation
q Flexible multipurpose UHV chamber
q Optimized for liquid jets and gas phase targets
q Up to for selectable hRIXS scattering angles (fixed)
q Vacuum protection: diff. pumping (to beamline) and
filters (to hRIXS)
q Collinear laser in-coupling
Tender awarded (Bestec GmbH)
Delivery scheduled for December 2018SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 27
TR-PES beamline at SASE3
Goal:
flexible spot size
30−100 µm (hor)
100 µm (ver)
344.5SASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 28
Experimental stations
Spin-filtering ToF Dual angle-resolving ToF
momentum microscopy photoelectron spectroscopy
(Univ. Mainz, G. Schönhense et al.) (Univ. Hamburg, W. Wurth et al.)
Load lock 4 3
Sample
manipulator
Prep
1
Photoemission chamber
2
chamber
Themis Themis
5 6
1000 1000 WAL
z
x
ω
7 X-rays y
!
© Lukas WenthausSASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 29
ToF momentum microscopy
ARTICLES NATURE MATERIALS DOI: 10.1038/NMAT4875
Achromatic
k-image 2.5 2.0 1.5 1.0 0.5 0 = EF
Energy dispersion
EB (eV)
10 ns
Spin filter
Zoom optics 1 Zoom optics 2
Sample Field-free drift section
Real-space image Delay-line
with field aperture detector (ns)
Medjanik et al.,
Nat.1 |Mater.
Figure 16, of615
Cross-section (2017)
the ToF k-microscope (lenses schematic) with calculated trajectories for 300 eV initial kinetic energy and 30 eV drift energy.
The achromatic k-image formed in the Fourier plane of the objective lens (top left inset) is dispersed in energy in the field-free drift section. An adjustable
field aperture (dashed circle)
acc
Mo (110)
1 in the real-space intermediate image (bottom inset, showing the elliptical footprint of the photon beam) defines the source
k = 4 Å @E
area. Thekfinal k-image is projected (with
kin = 1 keV
variable magnification) onto the detector via two zoom lenses and a narrow crossover at the entrance of the ToF
T = 30 K
spectrometer. The dots on the trajectories mark isochronous planes with 10 ns spacing. Right: E = constant sections at di�erent EB (taken at h⌫ = 447 eV).
⌦
The radial coordinate is stretched by a factor of 6.
3 An imaging spin filter can be shifted into the beam as denoted by an arrow.
y = 8 ⇥ 10 h⌫ = 447 · · · 574 eV
2⇡ Beamline P04, PETRA
Fourier plane of a special objective lens. Momentum distributions so kf runs through several repeated BZs III (Hamburg)
in the extended zone
with diameters up to 6 Å 1 (comprising up to 2.5 ⇥ 105 resolved scheme. The final states of the outgoing photoelectrons lie onSASE3 instruments – status and plans Serguei Molodtsov, January 24, 2018 30
Thank you for your attention
On behalf of
SQS - M. Meyer (Group Leader)
SCS - A. Scherz (Group Leader)
hRIXS - A. Föhlisch (Speaker)
TR-PES - K. Rossnagel (Speaker)You can also read
