Rennes OSU Analytical Common Centre (so-called CCA) - OSUR
←
→
Page content transcription
If your browser does not render page correctly, please read the page content below
Rennes OSU Analytical Common Centre (so-called CCA) Head: Aline Dia (+33 2 2323 5650 - aline.dia@univ-rennes1.fr) Table caption: laboratory/institution responsible for the analytical platform UMR ECOBIO UMR Géosciences Rennes UMR CReAAH UMR SAS Material Key words Analytical equipments Staff Applications manager Carbon, nitrogen, * CHN 2400 serie II Perkin Elmer Nathalie LE BRIS (IE- * Total element analysis in ecosystem phosphorus sulfur elemental analyzer (combustion CNRS) pools: soils, vegetals, sediments – size Microbiological activity under O2, oxidation on Cu column, Phone: + 33 2 2323 5079 level of sample : 40 mg maxi, Nutrients separation and catharometric Ecobio Office 223 Bât.14B * Total element analysis in ecosystem PLAY (Analytical Soils, waters, sediments detection), (To be renewed) pools: soils, vegetals, sediments – size Platform) * CS LECO elemental analyzer (direct Frédérique PALLOIS (T- level of sample : 350 mg maxi, combustion under O2, IR detection), UR1) * Nutrient analysis in waters and soil Heads : * Bran + Luebb AAIII continuous flux, Phone: + 33 2 2323 6150 solutions: N et P, Nathalie Le Bris Buchi mineralizer, Buchi distiller + Ecobio Office 223 * N different species analysis, organic UMR 6553 - (+ 33 2 2323 5079), titrator, Bât 14B and inorganic (Kjeldahl et Devarda * Bioritech dissolved organic carbon methods) – solutions and solid samples, Ecobio Hervé Colinet Analyzer (95°C persulfate oxidation), Marion CHORIN (IE-CNRS) * Analyse carbone organique soluble et (+ 33 2 2323 6438) * Corning 926 chlorimeter, Phone: + 33 2 2323 5427 biomasse microbienne du sol, * UV/Visible spectrophotometer Ecobio Office 223 Bât.14B * Organic and inorganic carbon analysis * Visible Versamax µ-slate reader in waters, * µ-slate reader + SAFAS cuvettes: * Choride analysis in waters, Visible UV, fluo * Nutrients assay, enzymatic and microbiological activities in waters and soil liquid extractions 1
2
Microbial biomass and * µ-GC SRA 3000 (Poraplot-U 6m, Nathalie LE BRIS (AI- * Gaseous release measurements linked microbiological activity, TCD), CNRS) to biological activities and microbial Organic matter * CP 9002 (Poraplot-Q 25m, FID), Phone: + 33 2 2323 5079 communities in gases and waters (CO2, decomposition, * µ-GC-MS (4 analysis paths TCD+MS) Ecobio Office 223 Bât.14B H2S, DMS), In and ex situ * Gaseous release measurements linked expérimentations Frédérique PALLOIS (T- to biological activities and microbial UR1) communities in gases and waters (CH4, Phone: + 33 2 2323 6150 PLFA), Ecobio Office 223 Bât 14B * Gaseous release measurements (C, N, S) : organic and mineral compounds in relation with soil and sediment microbiological activities Metabolites, pesticides *GC-MS Thermo with combiPal David Renault (MC-UR1) * Primary and secondary (sugars, amino Phone: + 33 2 2323 6627 acids, polyols, organic acids) metabolite Ecobio Office 238 Bât.14 analysis in various biological matrices (fauna and flora) UMR 6553 - * Pesticides analysis in soil extracts Ecobio Pesticides, metabolites * LC-MSMS Waters Acquity I Class Nathalie LE BRIS (AI- Pesticides and metabolites analysis in Xevo G2 XS Q ToF + GC CNRS) complex matrices Phone: + 33 2 2323 5079 Ecobio Office 223 Bât.14B Frédérique PALLOIS (T- UR1) Phone: + 33 2 2323 6150 Ecobio Office 223 Bât 14B 3
Chemical analyses Mineral chemical laboratory Cécile LE CARLIER DE Copper and bronze metallurgy Metal (Copper, Bronze) ICP-AES (Jobin Yvon 138 Ultrace) VESLUD (IE-CNRS) (Cu, Pb, Zn, Sb, Sn, Co, Ni, Bi, As, Ag, Fe, Ore Phone: + 33 2 2323 6716 Mn) Soils, slags, ceramics CReAAH office 18 Bât.24 Soil analyses (P, Fe3+/2+, Al3+, K+, Na+, Mg2+, Ca2+) Jean-Christophe Le BANNIER (T-CNRS) Phone: + 33 2 2323 5294 CReAAH office 223 Bât.24 Mineral chemistry Head : Cécile Le Carlier Chemical analyses Mineral chemical laboratory Mikaël GUIAVARC'H (T- Non organic samples. Elementary and UMR 6566 - de Veslud Metal (Copper, Bronze) Portable X Ray Fluorescence UR1) isotopic composition analysis. CReAAH (+ 33 2 2323 6716) Ore (NITON XL3T 950 Godd+) Phone: + 33 2 2323 5834 Source fingerprinting. Soils, slags, ceramics CReAAH office 223 Bât. Composition group identification. 24 Phosphorus concentration measurement in soils. Chemical analyses Mineral chemical laboratory Cécile LE CARLIER DE Non organic samples. Elementary and Metal (Copper, Bronze) LA-ICP-MS VESLUD (IE-CNRS) isotopic composition analysis. Source Ore (ICP Agilent 7700) Phone: + 33 2 2323 6716 fingerprinting. Composition group Soils, slags, ceramics (Laser CETAC LSX 213 G2) CReAAH office 18 Bât.24 identification. Ceramic manufacture technics. Laser granulometry * Laser granulometer Mikaël GUIAVARC'H (T- Archaeological material analysis Mineral sample X ray Diffractometry * X ray diffractometer (Rigaku UR1) preparation Mineral sample preparation : Miniflex) Phone: + 33 2 2323 5834 Polish sections manufacturing of rocks, rocks, sediments, ceramics, * Mineral sample preparation (saws, CReAAH office 223 Bât. ceramics, etc. UMR 6566 - slags swindler, polish machine, etc.) 24 CReAAH Head: Guirec Querré (+ 33 2 2323 5916) 4
Gas chromatography - * Organic chemistry laboratory Ramiro MARCH Identification and quantification of Mass Spectroscopy * Gas Chromatography (HP 6890) CR-CNRS organics: Fire and culinary technical Organic Mater/ * Gas Chromatography (HP 6850) + Phone: + 33 2 2323 5629 history, tool manufacturing technics Geochemistry MS (5975B) CReAAH office 201 Bât.24 Organic chemistry Anthropic and natural organic matter UMR 6566 - Jean-Christophe Le transfer (hydrocarbons, acids, sterols, Head: Ramiro March Organic components (acids, BANNIER T-CNRS cetones, etc.) CReAAH (+ 33 2 2323 5629) hydrocarbons, sterols, Phone: + 33 2 2323 5294 cetones, etc.) CReAAH office 223 Bât.24 Taphonomy and conservation of organic matter: chemical and isotopical signatures Wood * Dendrochronology laboratory Chantal LEROYER (IR- Dating, environmental context Charbons de bois * Xylology laboratory, anthracology MCC) restitution, organic material use, Pollens * Malacology and archaeozoology Vincent BERNARD (CR- livestock and food Shells and other marine laboratory CNRS) Dendrochronology animal remnants * Palynological extraction laboratory Véronique GUITTON (IR- Xylology Terrestrial animal bone INRAP) Anthracology remnants - Biological Optical microscopes Catherine DUPONT (CR- Palynology - Stereomicroscopes CNRS) Archaeozoology : mammals and marine - Dendrochronological measurement Anna BAUDRY (IR-INRAP) invertebrates Paleoenvironment, bench Cécile BRUN (MCF- vegetals and animals - Image analysis Nantes) UMR 6566 - Delphine BARBIER (IR- CReAAH Head: Chantal Leroyer INRAP) (+ 33 2 2323 5623) Laurent CHARRIEAU (T- CNRS) Hélène SEIGNAC (IE- INRAP) Nancy MARCOUX (IE- UR1) David AOUSTIN (IE-UR1) 5
Rock preparation → Diamond board chain sawing set Xavier LE COZ (T-UR1) Preparation of: Thin petrographic slides → Accutom 50 Struers-Isomet1000 Phone: + 33 2 2323 5914 -rock thin slides for petrographic studies Microprobe preparation Buhler precision saw Géosciences Rennes, -polished slides for microprobe chemical NanoSIMS preparation → PM5A Struers lapping group Office 001 Bât 5 analyses UMR 6118 - Vacuum condition → 20 Postes Brot grinding machine -thick slides for fluid inclusions study Géosciences impregnation → Tegrapol 25/Tégraforce5 polisher -nanoSIMS analysis -dedicated samples Rennes Thick slides system -BEM analysis-dedicated samples Polishing →Vaccum impregnation set – epoxy molding Rock crushing → Fritsch et Henri breaker crushers To be recruited (T-UR1 ) Sawing and préparation of mineral Sawing → Henri roll crusher Phone: samples Sieving → Bico disc crusher Géosciences Rennes 20 to 1000µm sieving Geomaterials: rock Powders for chemical → Fritsch planetary crusher Office Bât 5 Powder preparation for chemical UMR 6118 - preparation analyses → Diam 600 diamond chain saw analysis Géosciences → Diam 300 diamond saw Sand preparation for mineral separation Rennes → Rotap column siever (geochronology) Heads: Marc Jolivet (+ 33 2 2323 6746) and →Fall dispatcher Xavier Le Coz →D'Abiche mortar (+ 33 2 2323 5914) Mineral separation →Shaking table Yann LEPAGNOT (T-CNRS) Mineral separation for geochronology → Frantz isomagnetic separator Phone: + 33 2 2323 5789 and thermochronology → Carpco magnetic separator Géosciences Rennes → Densitest heavy mineral Office 125 Bât 15 concentrator →Mineral separation by heavy liquids UMR 6118 - (bromophorme, diiodomethane) Géosciences → DP-U Struers polisher Rennes → Minor Endescotts siever → Olympus SZ60 binocular microscope → Olympus BH metallographic microscope 6
Mass spectrometry CO2 laser probe coupled to an 39Ar- Dominique BAVAY (AI- 39 Ar-40Ar Geochronology 40 Rare gases Ar low background (inox) gas CNRS) Rare gas spectrometry 39 40 UMR 6118 - Ar- Ar extraction line and to a magnetic Phone: + 33 2 2323 3854 Head: Gilles Ruffet Géosciences Dating sector mass spectrometer dedicated Géosciences Rennes (+33 2 2323 5666) Rennes to rare gas analysis (MAP 215 Office 104 Bât.15 equiped with a Nier source) Mass spectrometry * VG SIRA 10 gas source mass Dominique BAVAY (AI- Isotopic geochemistry: isotopic analyses Gas source mass Stable isotopes (O, H, C) spectrometer CNRS) of rocks and fluids in geological and Fluid-rocks interactions * OPTIMA gas source mass Phone: + 33 2 2323 3854 environmental studies spectrometry (stable Environmental analyses spectrometer Géosciences Rennes isotopes) * O extraction line for oxides and Office 104 Bât.15 UMR 6118 - silicates Heads: Anne-Catherine Géosciences * O and C extraction line for Pierson-Wickmann carbonates Rennes (+33 2 2323 5056) and * H extraction line for minerals, rocks Philippe Boulvais and waters, as well as of C in organic (+33 2 2323 6179) matter * Extraction line for fluid inclusions Solid source mass Finnigan Mat 262 multicollector solid David VILBERT (T-CNRS) Concentrations and isotopic ratios spectrometry (TIMS) source mass spectrometry Phone : +33 2 2323 6508 determination, Rb-Sr, Sm-Nd and Pb-Pb Solid source mass Isotopic tracing multicollector + clean rooms for Géosciences Rennes methods on rocks, minerals, spectrometry Geochronology sample preparation Office 104 Bât.15 archaeological items, bioindicators (radiogenic isotopes) Radiogenic isotopes (lichens,etc.) and waters. UMR 6118 - Rb/Sr, Sm/Nd, U-Pb Dominique BAVAY (AI- U-Pb geochronology on single grain and Géosciences Heads: Marc Poujol Rocks, minerals, waters CNRS) Rb-Sr, Sm-Nd and Pb-Pb dating on Rennes (+33 2 2323 6208) Phone: + 33 2 2323 3854 minerals and whole rocks Géosciences Rennes Office 104 Bât.15 7
Thermochronology(*) Low-T thermochronology Zeiss M1m microscope David VILBERT (T-CNRS) Rocks dating by fission tracks and U-Th- Datation Imaging system/Fission track counting Phone : + 33 2 2323 6508 He Heads: Kerry Gallagher Fission tracks Sample preparation Géosciences Rennes (+ 33 2 2323 6208), U-Th-He He extraction line/ Office 104 Bât.15 Gilles Ruffet Geomorphology High résolution mass spectrometer UMR 6118 - (+ 33 2 2323 6085) and Rocks Dominique BAVAY (AI- Géosciences Marc Jolivet CNRS) Rennes (+ 33 2 2323 6746) Phone: + 33 2 2323 3854 (*) ongoing Géosciences Rennes development Office 104 Bât.15 U-Th-Pb Geochronology ICP-MS quadripôle Agilent 7700 Marc Poujol (MCF) U-Th-Pb datation of minerals (zircon, U-Th-Pb LA-ICP-MS équipé d’un pompage de l’interface Tél : + 33 2 2323 6208 monazite, xenotime, beddeleyite, Geochronology renforcé. Géosciences Rennes titanite, rutile) by laser ablation coupled Excimer 193 nm ESI laser Office 108/1 Bât.15 to ICP-MS « LA-ICP-MS ». UMR 6118 - (NWR193UC) entirely driven by Head: Géosciences computer and equipped by a European Union (FEDER) partly funded Marc Poujol Rennes Coherent laser. this equipment. (+33 2 2323 6208) 8
Organic matter fingerprinting Gas chromatography - Mass Emilie JARDE (CR-CNRS) Qualitative and quantitative analysis of Gas chromatography in recent environments spectrometer (GC-MS) Phone: +33 2 2323 5620 the lipidic and macromolecular fractions coupled to mass Molecular caracterisation Géosciences Rennes of environmental samples spectrometry Biomarker quantification Office 306/2 Bât.15 UMR 6118 - Head: Emilie Jardé Géosciences Marine LIOTAUD (IE- (+33 2 2323 5620) CNRS) Rennes Marine Liotaud Phone: +33 2 2323 5620 (+33 2 2323 5620) Géosciences Rennes Office 306/2 Bât.15 Present-day and fossil Frontier Lab pyrolyser coupled with a Laurent JEANNEAU (CR- Qualitative and quantitative analysis of macromolecule molecular GC-MS CNRS) macromolecule composition of different Thermochemiolysis compositions Phone: +33 2 2323 3969 environmental matrices (such as waters, Géosciences Rennes soils, sediments, etc.) and fossil ones Head: Office 327 Bât.15 (such as ambers, woods, etc.) UMR 6118 - Laurent Jeanneau Géosciences (+33 2 2323 3969) Marine LIOTAUD (IE- Rennes Marine Liotaud CNRS) (+33 2 2323 3969) Phone: +33 2 2323 5620 Géosciences Rennes Office 306/2 Bât.15 9
Atomic absorption Atomic absorption Flame/Furnace Patrice PETITJEAN (IE- Major and trace element analysis in Major and trace elements (Solaar M6 THERMO) CNRS) environmental studies Waters Phone: +33 2 2323 6087 Géosciences Rennes Office 303 Bât.14B Dissolved organic carbon Carbon analyzer (TOC 5050 Shimadzu) Patrice PETITJEAN (IE- Dissolved organic carbon (DOC) and (DOC) and inorganic carbon and ASI 5000A sampler CNRS) inorganic carbon (DIC) measurements in Elemental and (DIC) concentration Phone: +33 2 2323 6087 fresh solutions Molecular measurements Géosciences Rennes Geochemistry (GEM) Waters Office 303 Bât.14B Heads: Mathieu Pédrot (+33 2 2323 6083) and Ion chromatography Ion chromatography Major and trace inorganic anion assay UMR 6118 - Martine Bouhnik-Le Coz Major and (trace) élément (DIONEX DX 120) Géosciences (+33 2 2323 6082) concentration assay Rennes Waters Colorimetric assay Fe (II) UV/Visible (Uvikon XS- Biotek) Colorimetric assay (190 à 900 nm) (Fe Waters spectrophotometer (II), phosphates…) Titrations/ Alkalinity 4 automatic titrators (2 Titrino 719S, 1 Diverse titrations and alkalinity Titrino 702SM, 1 Titrino 794 Basic) measurement ICP-MS solution mode ICP-MS (Agilent technologies - 7700 Trace and nanotrace multielement and Quantitative analysis serie ICP-MS) some major cation analysis in Trace elements environmental studiesl: Major cations Martine BOUHNIK-LE COZ - fresh natural waters Fresh waters (IE-CNRS) - solution extraction during interaction Phone: +33 2 2323 6082 experimentation under controlled Géosciences Rennes conditions (Soil/Water/Bacteria) Office 302 Bât.14B On specific request for environmental and geological studies : vegetals, gems, minerals, biogenic materials, etc. 10
Ion Chromatography: major Dionex ICS 3000 Yannick FAUVEL (AI-INRA) major anions, cations and trace anions, cations and trace Ion Chromatography (Rennes) Phone: +33 (0) 223 485 elements in water samples elements 667 INRA Centre, Rennes UMR SAS 1069 - INRA Béatrice BLAIZE (TR-INRA) Rennes- Phone: +33 (0) 223 485 Quimper 665 INRA Centre, Rennes Colorimetric analysis Continuous Flow Analyzer Bran Lubbe Maryvonne LEROY (TR- Nitrogen and phosphorous mineral nitrogen, phosphorous (Quimper) INRA) forms in environmental samples (waters Continuous Flow Analyzer Alpkem RFA Phone : +33 (0)298 959 and soils) 300 (Rennes) 965 UV/Visible Spectrophometer Lamda INRA Centre, Quimper Analytical department 20 Perkin Elmer (Rennes) Digesteur and distiller Buchi (Rennes Laurence CARTEAUX (TR- UMR SAS Head: Yannick Fauvel et Quimper) INRA) (+ 33 2 2348 5667) 1069 - INRA Phone +33 (0) 223 485 424 Rennes- INRA Centre, Rennes Quimper Yannick FAUVEL (AI-INRA) Phone +33 (0) 223 485 667 INRA Centre, Rennes Atomic absorption: 3100 Perkin Elmer Atomic Absorption Maryvonne LEROY (TR- Major cation analysis in environmental major cations (Quimper) INRA) samples (waters) UMR SAS Phone: +33 (0)298 959 1069 - INRA 965 Rennes- INRA Centre, Quimper Quimper 11
Total carbon and nitrogen Elemental analyzer Flash EA 1112 Béatrice BLAIZE (TR-INRA) Elemental analyzer C et N (soils and UMR SAS analysis Thermofinnigan (Rennes) Tél : +33 (0) 223 485 665 vegetals) 1069 - INRA INRA Centre, Rennes Rennes- Quimper Fluorescence spectroscopy, LS55 Perkin Elmer Fluorescence Anne JAFFREZIC (MC- Organic matter qualitative analysis in Fingerprint, organic matter spectrometer (Rennes) Agrocampus) environmental analysis Tél : +33 (0)223 485 420 UMR SAS Rennes 1069 - INRA Rennes- Armelle RACAPE (TR- Quimper Agrocampus) Tél : +33 (0)223 485 424 Soil thin sections Production line for soil sections Vincent HALLAIRE (CR- Soil sections making of undisturbed soil making: water/acetone exchange, INRA) samples UMR SAS resin impregnation, sawing and INRA Centre, Rennes 1069 - INRA abrasive polishing (Logitech LP50) Yannick BENARD (TR- Rennes- Soil micromorphology INRA) Quimper INRA Centre, Rennes Head : Vincent Hallaire Porosity, image analysis Microscope, stereoscope, image Vincent HALLAIRE (CR- Morphological characterization of soil (+33 (0) 2 2348 5429) analyser INRA) sections using image analysis UMR SAS INRA Centre, Rennes 1069 - INRA Yannick BENARD (TR- Rennes- INRA) Quimper INRA Centre, Rennes 12
You can also read