Lake/Reservoir Nutrient Monitoring Sampling and Analysis Plan for 2021 - Wyoming Department of Environmental Quality Water Quality Division ...
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Lake/Reservoir Nutrient Monitoring Sampling and Analysis Plan for 2021 Wyoming Department of Environmental Quality Water Quality Division - Watershed Protection Program 1
Lake/Reservoir Nutrient Monitoring Sampling and Analysis Plan for 2021 Reviewed and Approved by: 4/20/202 _____________________________________________________________________________ Jillian Scott, Qa/Qc Officer 1 Date Wyoming Department of Environmental Quality 4/21/2021 __________________________________________________________________________________________________ Lindsay Patterson, Surface Water Quality Standards Supervisor Date Wyoming Department of Environmental Quality 4/22/2021 __________________________________________________________________________________________________ Jeremy Zumberge, Surface Water Monitoring Program Supervisor Date Wyoming Department of Environmental Quality 4/20/2021 __________________________________________________________________________________________________ Eric Hargett, Natural Resource Program Principal (project manager) Date Wyoming Department of Environmental Quality Additional Reviewers Date Jason Martineau, Natural Resource Analyst, Monitoring Program, WDEQ/WQD 4/14/2021 Chad Rieger, Natural Resource Analyst, Monitoring Program, WDEQ/WQD 4/14/2021 Triston Rice, Natural Resource Analyst, Monitoring Program, WDEQ/WQD 4/14/2021 i
TABLE OF CONTENTS BACKGROUND AND OBJECTIVES......................................................................................................................................................... 1 CREDIBLE DATA AND QAPP ................................................................................................................................................................ 1 STANDARD OPERATING PROCEDURES ................................................................................................................................................ 1 STUDY DESIGN ................................................................................................................................................................................... 1 Number and Location of Sample Sites .......................................................................................................................... 1 Study Duration and Sample Frequency ......................................................................................................................... 3 Monitoring and Access Permissions ............................................................................................................................. 3 Primary WDEQ/WQD Field Personnel and Data Interpreters ........................................................................................ 3 Sample Parameters and Methods ................................................................................................................................ 4 Equipment (Electronic) Calibration, Maintenance and Calibration Logs ........................................................................ 5 Data Recording ............................................................................................................................................................ 6 Sample Labeling ........................................................................................................................................................... 6 Corrective Actions ........................................................................................................................................................ 6 Laboratories ................................................................................................................................................................. 6 QUALITY ASSURANCE/QUALITY CONTROL (QA/QC) ............................................................................................................................ 7 Data Verification and Validation ................................................................................................................................... 7 Chain of Custody .......................................................................................................................................................... 7 Field Quality Control for Chemical and Biological Samples (QC) .................................................................................... 7 Data Quality Objectives and Reconciliation .................................................................................................................. 7 Field Audits .................................................................................................................................................................. 7 DATA MANAGEMENT AND ARCHIVAL................................................................................................................................................. 8 Data Management ....................................................................................................................................................... 8 Data Archiving.............................................................................................................................................................. 8 ANALYSIS ........................................................................................................................................................................................... 8 REFERENCES ...................................................................................................................................................................................... 9 FIGURES Figure 1 – Locations of the five reservoirs (red circles) selected for sampling in 2021 along with selected municipalities (black circles). .......................................................................................................................................................................................................... 2 ii
BACKGROUND AND OBJECTIVES The monitoring and water quality standards groups will embark on a ninth year of collecting nutrient and supporting data on lakes and reservoirs. The focus of this year's monitoring will be a) drinking water storage reservoirs and/or public reservoirs with high recreation uses for which limited or no nutrient data exist and b) Boysen Reservoir (WDEQ/WQD 2021). Data from this monitoring will be used to ascertain the status of nutrient conditions in these waters; to assist in development of numeric nutrient criteria protective of aquatic life, recreation and/or drinking water; and be used to determine whether these waters should be prioritized for protection and/or restoration as part of Wyoming’s Nutrient Strategy (http://deq.wyoming.gov/wqd/nutrient-pollution/resources/wyoming-nutrient-strategy/). Data collected on Boysen Reservoir will be used in conjunction with external data to i) verify predictions of cyanobacterial bloom densities from CyAN satellite imagery (https://www.epa.gov/water-research/cyanobacteria-assessment-network-cyan), ii) evaluate linkages between cyanobacterial composition and cyanotoxin production in Boysen Reservoir. CREDIBLE DATA AND QAPP All data are collected in accordance with the credible data law specified in the Wyoming Environmental Quality Act § 35- 11-103(c)(xix) and detailed in Chapter 1, Section 35 of the Wyoming Water Quality Rules and Regulations. This SAP is covered by the WDEQ Water Quality Division (WQD), Watershed Protection Program Monitoring Quality Assurance Program Plan (QAPP) (WDEQ/WQD 2021b). STANDARD OPERATING PROCEDURES All standard operating procedures (SOPs) referenced within this SAP are found within the Manual of Standard Operating Procedures for Sample Collection and Analysis (WDEQ/WQD 2021c). STUDY DESIGN Site Selection The following five public reservoirs are selected for monitoring in 2021 (Figure 1). Owner Category Reservoir Acres Latitude Longitude Public 1 Worthen Meadows Reservoir 98 42.700600 -108.925100 Public 2 Frye Lake 145 42.707500 -108.878900 Public 3 Lower Sunshine Reservoir 971 44.086770 -108.986800 Public 1 West Newton Lake 29 44.543590 -109.123710 Public BR Boysen Reservoir 19,560 43.367743 -108.175406 Number and Location of Sample Sites For reservoirs that have not been previously sampled, the number and locations of sample sites will be determined during the first sample period according to the sample site selection criteria in Table 1 based on the reservoir’s category (Category 1: 10-100 acres; Category 2: 101-500 acres; Category 3: 500+ acres; Category 3(LR): large reservoirs). For reservoirs that have been previously sampled, monitoring will take place at established sample sites that correspond with the minimum selection criteria in Table 1. For Boysen Reservoir (Category BR), monitoring will take place at existing site locations as described in Table 2. Monitoring will take place at the same sample sites for all sample events. 1
Figure 1 – Locations of the five reservoirs (red circles) selected for sampling in 2021 along with selected municipalities (black circles). 2
Table 1 – Sample site selection criteria for each reservoir size class. Category No. of Sites Site Location(s) 1 1 Open water pelagic – deepest location 2 1 Open water pelagic – deepest location 3 2 Deepest locations within the ‘lacustrine pelagic’ and ‘riverine-transitional pelagic’ zones. If there are multiple ‘riverine-transitional pelagic’ zones, then select the zone that receives the largest inflow into the lake. 3 (LR) 3 Deepest locations within the ‘riverine pelagic’, ‘transitional pelagic’ and ‘lacustrine pelagic’ zones. If there are multiple ‘riverine pelagic’ zones, then select the zone that receives the largest inflow into the lake. Table 2 – Sample sites for Boysen Reservoir. Site ID Site Name Latitude Longitude WYDEQ_RES_303 Fremont Bay 43.251675 -108.184722 WYDEQ_RES_304 Tough Creek Campground 43.325483 -108.160000 WYDEQ_RES_305 East Shore 43.365706 -108.148611 WYDEQ_RES_68 Cottonwood Bay 43.346903 -108.212772 WYDEQ_RES_71 LPD 43.411997 -108.176744 WYDEQ_RES_67 TPD 43.302967 -108.201836 WYDEQ_RES_64 RPD 43.277556 -108.186297 Study Duration and Sample Frequency The duration of lake sampling extends from April to October 2021. Each lake site will be sampled according to Table 4. Table 1 – Sample duration and frequency for lakes identified in Table 1. Reservoir Category Sample Period Sample Frequency Parameters Mid to Late-June (Spring) Once Chemical, Physical and Biological 1 ,2, 3, and 3 (LR) Mid July to Early August (Summer) Once Chemical, Physical and Biological Early to Mid-September (Fall) Once Chemical, Physical and Biological BR April through October Monthly Chemical, Physical and Biological Monitoring and Access Permissions For access to or across private lands, authorization will be sought according to the internal standard operating procedure (SOP) for Private Land Access and WDEQ/WQD Policy #5 WQD Private Property Access Procedures (Form B). Approved private property access only applies to designated WDEQ staff and does not extend to other personnel/parties who may wish to accompany WDEQ during sampling. Travel routes will be documented for all sites where private permission is required to access or cross private lands. Primary WDEQ/WQD Field Personnel and Data Interpreters Sampler Office Title Contact Information Tavis Eddy Lander, WY Natural Resource Analyst Ph: (307) 335-6957 tavis.eddy@wyo.gov Mike Wachtendonk Lander, WY Natural Resource Analyst Ph: (307) 335-6751 michael.wachtendonk@wyo.gov 3
Jason Martineau Sheridan, WY Natural Resource Analyst Ph: (307) 675-5632 jason.martineau@wyo.gov Chad Rieger Sheridan, WY Natural Resource Analyst Ph: (307) 675-5637 chad.rieger@wyo.gov Jeremy ZumBerge Sheridan, WY Monitoring Program Supervisor Ph: (307) 675-5638 jeremy.zumberge@wyo.gov Triston Rice Cheyenne, WY Natural Resource Analyst Ph: (307) 777-6353 triston.rice@wyo.gov Eric Hargett Cheyenne, WY Natural Resource Program Principal Ph: (307) 777-6701 eric.hargett@wyo.gov Lindsay Patterson Cheyenne, WY Surface Water Quality Standards Ph: (307) 777-7079 Supervisor lindsay.patterson@wyo.gov Sample Parameters and Methods Parameter Sample Method / Sample Depth Reporting Analytical Preservative Holding Reporting SOP From Water Units RU Method Time Limit (same Surface units as RU) Chemical Alkalinity, Total Grab/ See SOP for 0.5 m mg/L SM2320B Iced to
pH See SOP for pH Entire Vertical S.U. SM4500-H+B None; FM N/A 0.01 Profile (See Lake/Reservoir Field Data Form) **Phosphorus, Grab / See SOP for 0.5 m µg/L EPA 365.1 Filter (0.45µm), 48 hours 5.0 Orthophosphate Chemical Grab Iced to
Conductivity At least once weekly At least once daily before Re-condition according See SOP for Instrument with either 100 or the first sample event to owner’s manual. Calibration and 1000 µS/cm standard with 100 or 1000 µS/cm Remove precipitate / Calibration Logs (see owner’s manual) standard debris Dissolved oxygen At least once weekly At least once daily Re-condition according See SOP for Instrument (DO) or with each 500 ft before the first sample to owner’s manual. Calibration and change in elevation event with water Remove precipitate / Calibration Logs (see owner’s manual) saturated air at a known debris and keep probe barometric pressure bulb moist Temperature, An annual check None Remove precipitate / See SOP for Instrument Water against a reference debris Calibration and thermometer (NIST) Calibration Logs Oxidation pH calibration is None Re-condition See SOP for Instrument Reduction sufficient for ORP according to owner’s Calibration and Potential (ORP) calibration manual. Remove Calibration Logs precipitate / debris and keep probe bulb moist Data Recording All data and information collected in the field will be recorded on official WDEQ/WQD electronic datasheets and/or the Lake/Reservoir Field Data Form that can be found at the back of this SAP. In some circumstances, field notebooks may also be used in addition to the Lake/Reservoir Field Data Form or electronic datasheets. Samples for laboratory analysis will be recorded on official chain of custody forms (see SOP for Chain of Custody). Sample Labeling See SOPs for Phytoplankton-Vertical Tow and Van Dorn Sample Method (attached), Chlorophyll (Lentic), and Sample Labeling. Corrective Actions Project evaluation will occur periodically during the sampling schedule outlined in this SAP. Necessary revisions may include but are not limited to site locations, sample methods and logistics, field forms and sampling logistics. Any revisions will be included as amendments to this SAP. The project manager will notify all associated field personnel, landowners and partners of amendments to this SAP along with implementation of any corrective actions. Laboratories The following laboratories will provide analytical services for samples collected as part of the project described in this SAP: 1. Wyoming Department of Environmental Quality, Water Quality Division Laboratory (WQD lab) The WQD lab will be the provider of analytical services for all water chemistry samples (excluding orthophosphate) collected as part of this project by WQD staff. The WQD lab will provide customized packages of bottles, labels, preservatives, and chain of custody forms prior to samples being collected as requested by samplers. Samplers will send samples to the WQD lab within one week of collection using United Parcel Service, Federal Express or 6
hand delivery. The WQD lab will analyze samples in accordance with established standards for holding time, analytical method, and data quality assurance and control. The WQD lab will follow the Watershed Protection Program standard operating procedures (WDEQ/WQD 2021c) and QAPP (WDEQ/WQD 2021b). 2. Rhithron Associates (Rhithron) Rhithron will provide taxonomic identification services for phytoplantkon samples collected as part of this project. Rhithron has provided taxonomic services to the Watershed Program since 2004 and is under contract through June 30, 2022. Preserved phytoplankton samples will be sent to Rhithron at the end of the field season. Rhithron will provide results to samplers within 90 days of receipt of samples. Rhithron will subsample, sort and identify specimens according to contract terms. Established standards for taxonomic identification will be followed. 3. Energy Laboratories, Casper Wyoming Energy Laboratories will be the provider of analytical services for orthophosphate samples collected as part of this project by WQD staff. Energy Laboratories will provide customized packages of bottles, labels, preservatives, and chain of custody forms prior to samples being collected as requested by samplers. A copy of the chain of custody used by Energy Laboratories is included in the back of this SAP. Samplers will send samples to Energy Laboratories within one week of collection using United Parcel Service, Federal Express or hand delivery. Energy Laboratories will analyze samples in accordance with established standards for holding time, analytical method, and their own data quality assurance and control procedures. QUALITY ASSURANCE/QUALITY CONTROL (QA/QC) Data Verification and Validation See SOPs for Data Validation and Data Verification as well as the Watershed Protection Program Monitoring Quality Assurance Program Plan (QAPP) (WDEQ/WQD 2021b). Chain of Custody See SOP for Chain of Custody. Field Quality Control for Chemical and Biological Samples (QC) Field Qc Samples Collection Frequency Parameters Field Blank At least 10% for all collected samples (Chemical) All listed, except FM Duplicate At least 10% for all collected samples (Chemical and Biological) All listed See SOP for Blanks and Quality Control Measures, Summary Of; FM = Field Measurement Data Quality Objectives and Reconciliation Data collected under this SAP will be evaluated by the Qa/Qc Officer with respect to the data objectives listed in this SAP and data quality objectives identified in the WDEQ/WQD SOP for Precision and the QAPP (WDEQ/WQD 2021b). If it is determined that one or more data objectives/components were not met, the project manager will be informed and given an opportunity to provide justification to the Qa/Qc Officer as to whether the particular data objective/component should be qualified or rejected and if future data components/objectives should be altered. Field Audits A field audit by the WDEQ/WQD QA/QC Officer will be accommodated if requested. 7
DATA MANAGEMENT AND ARCHIVAL Data Management Data Type Storage Location Chemical WDEQ/WQD Nutrient Database, spreadsheet and .pdf WDEQ/WQD Cheyenne, Lander and Sheridan Biological, Chlorophyll-a WDEQ/WQD Nutrient Database and Algal Database, spreadsheet and WDEQ/WQD Cheyenne, .pdf Lander and Sheridan Biological, Phytoplankton Algal Database, spreadsheet and .pdf WDEQ/WQD Cheyenne, Lander and Sheridan Physical WDEQ/WQD Nutrient Database, spreadsheet and .pdf WDEQ/WQD Cheyenne, Lander and Sheridan Data Archiving Data Item Format Backup Copy & Format Location Retention Field Data Sheets Electronic (.pdf, .xlsx, other) Electronic (.pdf) WDEQ/WQD Cheyenne, Permanent & paper Lander and Sheridan Photographs Electronic (.jpg) Electronic (.jpg) WDEQ/WQD Cheyenne, Permanent Lander and Sheridan Field Log Books Paper Electronic (.pdf) WDEQ/WQD Cheyenne, Permanent Lander and Sheridan Laboratory Results/Qa Electronic (.csv, .docx and Electronic (.csv, .docx and WDEQ/WQD Cheyenne, Permanent pdf) pdf) Lander and Sheridan Agency Qa Reports Electronic (.docx and .pdf) Electronic (.docx and .pdf) WDEQ/WQD Cheyenne, Permanent Lander and Sheridan Calibration Logs Electronic (.jpg) and paper Electronic (.pdf) WDEQ/WQD Cheyenne, Permanent Lander and Sheridan Chain of Custody Electronic (.xlsx and .pdf) and Electronic (.xlsx and .pdf) WDEQ/WQD Cheyenne, Permanent paper Lander and Sheridan Spreadsheets, other Electronic (.xlsx, .txt, .dbf, Electronic (.xlsx, .txt, .dbf, WDEQ/WQD Cheyenne, Permanent electronic files other) other) Lander and Sheridan Database Electronic (.mdb, other) Electronic (.mdb, other) WDEQ/WQD Cheyenne, Permanent Lander and Sheridan Reports, emails, Electronic (.wpd, .pdf, .html) Electronic (.docx, .pdf and WDEQ/WQD Cheyenne, Permanent letters & paper .html) Lander and Sheridan -All records are the property of the State and therefore subject to the Wyoming Public Records Act. -Records may be transferred to the Wyoming State Archives according to procedures in the State Agency Crosswalk Schedule. ANALYSIS Analytical methods that could be used for development of nutrient criteria using data collected pursuant to this project and other data sources include but are not limited to those identified in the Wyoming Nutrient Criteria Development Plan (WDEQ/WQD 2018b). Data analysis efforts to accomplish identified objectives specific to Boysen Reservoir will be conducted by a third-party under a separate sampling and analysis plan approved by the WDEQ. 8
REFERENCES WDEQ/WQD. 2021a. Water Quality Monitoring Plan. Wyoming Department of Environmental Quality, Water Quality Division, Watershed Protection Program, Sheridan, Wyoming. WDEQ/WQD. 2021b. Quality Assurance Project Plan (QAPP) for Watershed Protection Program Water Quality Monitoring. Wyoming Department of Environmental Quality, Water Quality Division, Cheyenne, Wyoming. WDEQ/WQD. 2021c. Manual of Standard Operating Procedures for Sample Collection and Analysis. Wyoming Department of Environmental Quality, Water Quality Division, Cheyenne, Wyoming. WDEQ/WQD. 2018a. Wyoming Water Quality Rules and Regulations – Chapter 1. Wyoming Department of Environmental Quality, Water Quality Division, Cheyenne, Wyoming. WDEQ/WQD. 2018b. Wyoming Nutrient Criteria Development Plan. Wyoming Department of Environmental Quality, Water Quality Division, Cheyenne, Wyoming. 9
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WYOMING DEPARTMENT OF ENVIRONMENTAL QUALITY LAKE/RESERVOIR FIELD DATA FORM LAKE/RESERVOIR DESCRIPTION (Complete Bold and Underlined Entries in Field) DATE (mm-dd-yyyy) __ __ - __ __ - __ __ __ __ DEQ ID CODE __ __ __ __ __ __ __ MAJOR BASIN_____________________ WATERBODY NAME ________________________________________________________________________________________ SAMPLE SITE LOCATION (Check one location): Deepest Region Riverine-Transitional Zone - Pelagic Lacustrine Zone - Pelagic Riverine Zone- Pelagic Transitional Zone- Pelagic Lacustrine Zone- Littoral Riverine Zone- Littoral Transitional Zone- Littoral Other (Embayment, Tributary Inflow):_______________________________________________________________________________________ SAMPLING PURPOSE/PROJECT: Reference Random Targeted Spill/Complaint Other_______________________________ DATA COLLECTORS (and initials) _______________________________________________________________________________ Note: List all observers by name in the Field Notes. HUC CODE __ __ __ __ __ __ __ __ __ __ __ __ DEQ SURFACE WATER CLASSIFICATION: 1 2 2ww 3 4 AB A B C D Class Subcategory ECOREGION: Level III________________________________________ Level IV_________________________________________ USGS MAP (1:24K) _______________________________________ BLM MAP (1:100K) _____________________________________ COUNTY _____________________________ COORDINATES ____1/4____1/4 SEC___ ___ T___ ___N R___ ___ ___W GPS FIELD FILE _______ LATITUDE __ __. __ __ __ __ __ __ __ __ __ LONGITUDE __ __ __. __ __ __ __ __ __ __ __ __ ELEVATION ____________ft SURFACE AREA ___________ac (Circle one): Maximum Pool Normal Pool Minimum Pool DRAINAGE AREA ____________mi2 LANDFORM (Circle one): Mountain Foothills Plains LAND STATUS (Circle one): Private State County Municipal Military Tribal USFS BLM USFWS NPS DOE BOR CONTACT ______________________________________________________________ PHONE (_____) _____ - _____________ ADDRESS __________________________________________________________________________________________________ RESULTS REQUESTED? Y N Notes: ___________________________________________________________________ DIRECTIONS TO WATERBODY: _____________________________________________________________________________ ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ PRIMARY LAND USE (Circle one), SECONDARY LAND USE (Circle one & label #2) and LESSER LAND USES (Underline) within immediate vicinity of shoreline. Non-irrigated Hayland Irrigated Hayland Non-irrigated Row Crop Irrigated Row Crop Livestock Grazing Confined Feedlot Logging Industrial Urban Military Reserve Mining Oil & Gas Recreation & Wildlife Habitat Other_______________________________ PRESENT ON OR UPSTREAM OF WATERBODY? (Circle all that apply): Irrig. Diversion Irrig. Return Municipal Intake Dam Causeways Road Crossings Connected Roads Channel Alteration (i.e., dredged, artificial embankments, concrete lined) Boat Launches Campgrounds Swimming Beaches Summer Residences Permanent Residences Beaver Dams Fish Habitat Structures Fish Habitat Structures FLOW AUGMENTATION? (Circle all that apply): None Point Discharge(s) Trans-Basin Flow Diversion Irrigation Return Artesian/Well(s) Revised 3/26/2020 - 11 -
WYOMING DEPARTMENT OF ENVIRONMENTAL QUALITY LAKE/RESERVOIR FIELD DATA FORM LAKE/RESERVOIR DESCRIPTION (Continued) POINT SOURCE DISCHARGES: List name, permit number, and type (i.e., WWTF, oil treater, industrial) that discharge to waterbody and its tributaries. Estimate distance from outfall to waterbody. List additional facilities in the Field Notes. DISTANCE % FLOW FACILITY NAME PERMIT NO. TYPE (Stream Miles) CONTRIBUTION DESCRIBE AND PHOTO-DOCUMENT SOURCES OF POLLUTANTS VISIBLY CONTRIBUTING TO WATER QUALITY CHANGE (i.e., point sources, urban runoff, connected disturbed areas and roads, road crossings):_____________________________ ___________________________________________________________________________________________________________ DESCRIBE NATURAL FACTORS VISIBLY CONTRIBUTING TO WATER QUALITY CHANGE (i.e., highly erosive soils, geologic features, springs, thermal features): _____________________________________________________________________ ___________________________________________________________________________________________________________ DESCRIBE BEST MANAGEMENT PRACTICES (BMP’s) IN PLACE TO CONTROL NPS POLLUTANTS: ____________ ___________________________________________________________________________________________________________ BEDROCK GEOLOGY (Love and Christiansen 1985)_____________________________________________________________________ ____________________________________________________________________________________________________________ PREDOMINANT SOIL TYPE ________________________________________________________________ (NRCS County Soil Survey) __________________________________________________________________________________________ (Munn and Arneson 1998) GENERAL OBSERVATIONS WEATHER CONDITIONS ________________________________________________________________________________________________ Any recent runoff due to precipitation or snow melt? Y N If yes, within how any days? (Circle all that apply): 1 2 3 4 5 >5 WATER SHEEN SLIMES COLOR ODORS □ None □ None □ None □ None □ Intermittent □ Rare □ Brown □ Anaerobic □ Consistent □ Common □ Green □ Sewage □ Free Product □ Abundant □ Gray □ H2S □ Other_____________________ □ Other_____________________ SECCHI DISK TRANSPARENCY TIME _________ CLOUD COVER _________ % SURFACE WATER CONDITIONS _________________________________ NO. 1: Disappears @ _________ m Reappears @ _________ m NO. 2: Disappears @ _________ m Reappears @ _________ m AVERAGE TRANSPARENCY DEPTH ___________ m TOTAL WATER DEPTH AT SAMPLE SITE _____________________ m CHLOROPHYLL α DATE (mm-dd-yyyy) __ __ - __ __ - __ __ __ __ TIME ____________ SAMPLE ID ___ ___ ___ - ___ ___ - ___ ___ ___ - ____C (Initials) - (Year) - (J. day) - (No.) COLLECTION DEPTH __________ m QA DUPLICATE? Y N DUPLICATE ID ___ ___ ___ - ___ ___ - ___ ___ ___ - ____C SAMPLE VOLUME FILTERED ________ mL FILTER MESH SIZE 0.7 µ Other?______ µ PRESERVED (Ethanol/Other)? Y N Revised 3/26/2020 - 12 -
WYOMING DEPARTMENT OF ENVIRONMENTAL QUALITY LAKE/RESERVOIR FIELD DATA FORM PHYTOPLANKTON DATE (mm-dd-yyyy) __ __ - __ __ - __ __ __ __ TIME _______ SAMPLE ID ___ ___ ___ - ___ ___ - ___ ___ ___ - ____PLV or PLN (Initials) - (Year) - (J. day) - (No.) COLLECTION DEPTH __________ m QA DUPLICATE? Y N DUPLICATE ID ___ ___ ___ - ___ ___ - ___ ___ ___ - ____PLV or PLN NET MESH SIZE: 76 µm Other _____ µm TOTAL WATER DEPTH: _______________________ m ESTIMATED MAXIMUM WATER FILTERED (Vm) __________ L Vm = [a0.0652 * SAMPLE DEPTH * 3.1416 * 1000] INITIAL SAMPLE VOLUME _______mL LUGOL’S PRESERVATIVE VOLUME _______mL TOTAL SAMPLE VOLUME _______mL aWisconsin® Plankton Net Mouth Radius = 0.065 m WATER SAMPLES DATE (mm-dd-yyyy) ___ ___ - ___ ___ - ___ ___ ___ ___ QA DUPLICATE? Y N Surface Sample ID ___ ___ ___ - ___ ___ - ___ ___ ___ - ___ S Duplicate Surface Sample ID ___ ___ ___-___ ___-___ ___ ___-___ S (Initials) - (Year) - (J. day) - (No.) (Initials) - (Year) - (J. day) - (No.) Bottom Sample ID ___ ___ ___ - ___ ___ - ___ ___ ___ - ___ B Duplicate Bottom Sample ID ___ ___ ___-___ ___-___ ___ ___-___ B Location Time Parameter Container Preservative Preserved? Alkalinity □ 500 mL P □ Other ____________ I Y N [Total N (TN)] [Nitrate+Nitrite N] [Ammonia-N] □ 500 mL P □ Other ____________ 1+1 H2SO4, I Y N ________ [Total Phosphorus (TP)] □ 500 mL P □ Other ____________ 1+1 H2SO4, I Y N Surface _______ Depth (m) [Orthophosphate P] □ 500 mL P □ Other ___________ I Y N [Total Microcystin Nodularin] [Cylindrosperrmopsin] □ 60 mL PETG Amber P □ Other___ I Y N 3mL 10x [Anatoxin-a] [Saxitoxin] □ 40 mL Amber G □ Other ________ Diluent, I Y N Alkalinity □ 500 mL P □ Other ____________ I Y N [Total N (TN)] [Nitrate+Nitrite N] [Ammonia-N] □ 500 mL P □ Other ____________ 1+1 H2SO4, I Y N ________ [Total Phosphorus (TP)] □ 500 mL P □ Other ____________ 1+1 H2SO4, I Y N Bottom _______ Depth (m) [Orthophosphate P] □ 500 mL P □ Other ____________ I Y N [Total Microcystin Nodularin] [Cylindrosperrmopsin] □ 60 mL PETG Amber P □ Other___ I Y N 3mL 10x [Anatoxin-a] [Saxitoxin] □ 40 mL Amber G □ Other ________ Diluent, I Y N E. COLI DATE (mm-dd-yyyy) __ __ - __ __ - __ __ __ __ TIME ____________ COLLECTION DEPTH __________ m CONTAINER: IDEXX Whirl-Pak Other________ QA DUPLICATE? Y N VOLUME: 100 mL Other__________mL BLANK PREPARED: Y N TIME BLANK PREPARED ___________ SAMPLES PRESERVED ON ICE? Y N Revised 3/26/2020 - 13 -
WYOMING DEPARTMENT OF ENVIRONMENTAL QUALITY LAKE/RESERVOIR FIELD DATA FORM FIELD/LAB INSTRUMENTS USED (Include Model and Serial Numbers) pH: DISSOLVED OXYGEN: _____________________________________________________________ ____________________________________________ TEMPERATURE: CONDUCTIVITY: _________________________________________________ _________________________________________________ VERTICAL PROFILE MEASUREMENTS For depths 3 meters, record measurements at: * the surface; and * 1.0 meter intervals down to 15 meters; and * 5.0 meter intervals from 15 to 30 meters; and * 10.0 meter intervals below 30 meters to a depth 1.0 meter above the bottom. Data File Name ______________________________________________________________________________________________ Temp Cond Temp Cond Depth D.O. D.O. Depth D.O. D.O. (µS/cm (µS/cm (m) Time (C) pH (mg/L) (%) ORP (m) Time (C) pH (mg/L) (%) ORP ) ) Surface 11 0.5 12 1.0 13 1.5 14 2.0 15 2.5 20 3 25 4 30 5 40 6 50 7 60 8 70 9 80 10 90 Revised 3/26/2020 - 14 -
WYOMING DEPARTMENT OF ENVIRONMENTAL QUALITY LAKE/RESERVOIR FIELD DATA FORM INSTRUMENT CALIBRATION CHECK (performed after field sample measurements are made) Instrument Calibration Date1 Value of Check Standard Measured Value of Check Standard pH (S.U.) Sp. Cond. (µ S/cm @ 25ºC) Dissolved Oxygen (% satn.) Not applicable Not applicable 1Refer to field sampler’s instrument calibration log book. QA/QC ITEMS WATER QUALITY TRIP BLANK? Y N TRIP BLANK SAMPLE ID ___ ___ ___ - ___ ___ - ___ ___ ___ - ____ WATER QUALITY FIELD BLANK? Y N FIELD BLANK SAMPLE ID ___ ___ ___ - ___ ___ - ___ ___ ___ - ____ Field form checked for completeness by (print full name): _______________________________________________ Date: _____________ Calculations performed by (print full name): _________________________________________________________ Date: _____________ Calculations checked by (print full name): ___________________________________________________________ Date: _____________ FIELD NOTES ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ ____________________________________________________________________________________________________________ Revised 3/26/2020 - 15 -
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