Construction and commissioning of the - Horizon 2020 research and innovation programme Project: No 690323 SMART-Plant
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This project has received funding from the European Union’s Horizon 2020 Ref. Ares(2017)4843381 - 04/10/2017 research and innovation programme under grant agreement No. 690323 Horizon 2020 research and innovation programme Project: No 690323 SMART-Plant Full project title: Scale-up of low-carbon footprint material recovery techniques in existing wastewater treatment plants (SMART-Plant) DeliverableD3.2 Construction and commissioning of the SidestreamSMARTechs Due date of deliverable: 31 May 2017 Actual submission date: 04 Oct 2017
Project: No 690323 DOCUMENT INFORMATION: Construction and commissioning of the Deliverable Number D3.2 Title: Sidestream SMARTechs Work Package Number WP3 Title: Side- and Down-stream SMARTechnologies Due date of deliverable Contractual M6 Actual M6 Version number 1.0 Format Pdf file Creation date 15/05/2017 Version date 20/09/2017 Type R DEM DEC OTHER ETHICS Dissemination Level PU Public CO Confidential Rights Copyright “SMART-Plant Consortium”. During the drafting process, access is generally limited to the SMART-Plant Partners. Responsible author Paolo Pozzato, Davide pozzato@scaevicenza.it; Name: Savio, Monica E-mail: tecnico@scaevicenza.it, Miglioranza segreteria@scaevicenza.it Partner: SCAE Phone: +39 0444 360 533 Other authors Constantinos Noutsopoulos, Simos Malamis, Daniel Mamais, Name: Partner: NTUA Andreas Andreadakis, Evangelos Statiris Name: Nicola Frison, David Bolzonella Partner: UNIVR Name: Daniele Renzi Partner: ATS SMART-Plant D3.2
Project: No 690323 Ioanna Droubogianni, Dimitra Name: Kollia, Panagiotis Lalis, George Partner: AKTOR Zarras Brief Description Deliverable 3.2 is part of WP3 which is related to side- and down-stream SMARTechnologies. More specifically D3.2 focuses in three sidestream SMARTechnologies that are integrated in the existing conventional sewage sludge treatment line to provide more energy efficiency for the i) removal of nitrogen, ii) recovery of phosphorus and iii) recovery of PHA. The D3.2 is to the construction and the commissioning of the sidestream SMARTechs. Keywords sidestream Smartechs, construction, commissioning Version log Revision history Rev. No. Issue Date Modified by Comments Minor revision by Coordinator before Version 1 03/10/2017 Francesco Fatone submission SMART-Plant D3.2
Project: No 690323 TABLE OF CONTENTS Document Information: ......................................................................................................................... 2 Table of Contents ................................................................................................................................... 4 List of Tables .......................................................................................................................................... 5 List of Figures ......................................................................................................................................... 5 Executive Summary................................................................................................................................ 6 Abbreviations ......................................................................................................................................... 9 1. Introduction ............................................................................................................................. 11 2. SMARTech4a - Sidestream SCENA ........................................................................................... 13 2.1 Technical description of the SMARTech 4A ............................................................................. 13 2.2 List of the electromechanical equipment ................................................................................ 16 2.3 Practical instructions for the operation of SMARTech 4A ....................................................... 23 2.1 Integrability of the Smartech 4a in existing WWTPs ............................................................... 25 2.2 Drawings ‘as built’ .................................................................................................................... 27 2.3 Picture report ........................................................................................................................... 28 3. SMARTech4b - Sidestream THERMAL HYDROLYSIS-SCENA ..................................................... 32 3.1 Technical description of the SMARTech 4B ............................................................................. 32 3.2 List of the electromechanical equipment ................................................................................ 35 3.3 Practical instructions for the operation of SMARTech 4B ....................................................... 39 3.1 Integrability of the Smartech 4b in existing WWTPs ............................................................... 42 3.2 Drawings ‘as built’ .................................................................................................................... 44 3.3 Pictures report ......................................................................................................................... 44 4. SMARTech5 - Sidestream SCEPPHAR ....................................................................................... 52 4.1 Technical description of the SMARTech 5 ............................................................................... 52 4.1 List of the electromechanical equipment ................................................................................ 54 4.2 Practical instructions for the operation of SMARTech 5 ......................................................... 66 4.3 Integrability of the Smartech 5 in existing WWTPs ................................................................. 72 4.4 Drawings ‘as built’ .................................................................................................................... 74 4.5 Pictures report ......................................................................................................................... 74 SMART-Plant D3.2
Project: No 690323 LIST OF TABLES Table 1 Specification of the grinder for the mixed primary sludge. .................................................... 16 Table 2 Specification for the installation of the dynamic thickening .................................................. 16 Table 3 Specification of the fermentation unit.................................................................................... 18 Table 4 Specification for the installation of the screw-press separator for the mixed sludge fermentation ........................................................................................................................................ 19 Table 5 Specification of the Short-Cut Sequencing Batch Reactor ...................................................... 19 Table 6 Operation of the fermentation unit ........................................................................................ 23 Table 7 Operation of the screw-press separator ................................................................................. 24 Table 8 Operation of the short-cut Sequencing Batch Reactor. .......................................................... 25 Table 9 Major units and specifications of the electro-mechanical equipment ................................... 36 Table 10 Basic features of automation in the operation of pilot plant system. .................................. 40 Table 11 List of electromechanical equipment and FLOW DIRECTION of the Salsnes Filter .............. 54 Table 12 List of tanks, electromechanical equipment, sensors and FLOW DIRECTION of the Sequencing Batch Fermentation Reactor ............................................................................................ 55 Table 13 List of tanks, electromechanical equipment, sensors and flow direction of the ultrafiltration unit ....................................................................................................................................................... 57 Table 14 Specification of the crystallization unit ................................................................................. 57 Table 15 List of tanks, electromechanical equipment, sensors and flow direction of the nitritation unit .............................................................................................................................................................. 59 Table 16 List of tanks, electromechanical equipment, sensors and flow direction of the PHA- accumulating biomass selection SBR ................................................................................................... 61 Table 17 List of tanks, electromechanical equipment, sensors and flow direction of the accumulation SBR ....................................................................................................................................................... 64 Table 18 Operation of the SF1000 ....................................................................................................... 66 Table 19 Operation of the fermentation unit ...................................................................................... 67 Table 20 Operation unit of the ultrafiltration unit .............................................................................. 68 Table 21 Operation of the crystallizer ................................................................................................. 68 Table 22 Operation of the nitritation unit ........................................................................................... 70 Table 23 Operation of the selection SBR ............................................................................................. 71 Table 24 Operation of the accumulation SBR ...................................................................................... 72 LIST OF FIGURES Figure 1 Deliverables of WP3 related to sidestream SMARTechs. ...................................................... 11 Figure 2 P&id of the Smartech 4a ........................................................................................................ 13 Figure 3 SMARTech 4a - Dynamic thickener of the sewage sludge ..................................................... 28 Figure 4 SMARTech 4a – Screw-press for S/L of the fermentation sewage sludge............................. 28 Figure 5 SMARTech 4a – Accumulation tank for the fermentation liquid of mixed sludge ................ 29 Figure 6 SMARTech 4a – Different views of the fermentation ............................................................ 29 Figure 7 SMARTech 4a - Electrical Panel and air compressor of Smartech 4a .................................... 30 SMART-Plant D3.2
Project: No 690323 Figure 8 SMARTech 4a -Tank for the acculation of the anaerobic supernatant and influent pump of the scSBR .............................................................................................................................................. 30 Figure 9 SMARTech 4a - Air diffusion system of the scSBR ................................................................. 31 Figure 10 Flow diagram of Psittalia WWTP with SMARTech 4b .......................................................... 32 Figure 11 Major units of SMARTech 4b and their interconnections ................................................... 33 Figure 12. Plan view of SMARTech 4B ................................................................................................. 44 Figure 13 Plan view of SMARTech 4B .................................................................................................. 45 Figure 13 3D drawing of SMATech 4B ................................................................................................. 45 Figure 15 SMARTech 4B – construction phase .................................................................................... 46 Figure 16 SMARTech 4B – construction phase .................................................................................... 46 Figure 17 SMARTech 4B – construction phase – installation of reject water storage tanks............... 47 Figure 18 SMARTech 4B – construction of raw and treated reject water networks ........................... 47 Figure 19 SMARTech 4B – overview of feed pump, decanting pump and decanting network ........... 48 Figure 20 SMARTech 4B – overview of feed pump and decanting pump ........................................... 48 Figure 21 SMARTech 4B – decanting system ....................................................................................... 49 Figure 22 SMARTech 4B – chemicals and substrate dosing pumps .................................................... 49 Figure 23 SMARTech 4B – chemicals and substrate storage tanks ..................................................... 50 Figure 24 SMARTech 4B – installation of on-line probes .................................................................... 50 Figure 25 SMATech 4B – hydraulic testing of the SBR ......................................................................... 51 Figure 26 SMATech 4B –testing of the aeration system of the SBR .................................................... 51 Figure 27 P&id of the Smartech 5. ....................................................................................................... 52 Figure 28 SMARTech 5 - Integrated container with rotating belt filter intalled ................................. 74 Figure 29 SMARTech 5 - Hopper for the cellulosic primary sludge .................................................... 75 Figure 30 SMARTech 5 - Installation of the Smartech 5 ...................................................................... 75 Figure 31 SMARTech 5 - (a) Sequencing Batch Fermentation Reactor during the installation; (b) Sequencing Batch Fermentation Reactor placed in the platform ....................................................... 76 Figure 32 Ultrafiltration unit ................................................................................................................ 76 Figure 33 SMARTech 5 - Ultrafiltration system (right side) and crystallizer (right side) ..................... 77 Figure 34 SMARTech 5 - Left side,Nitritation, Selection and Accumulation SBRs; Right side, ultrafiltration system and cristallizer. .................................................................................................. 77 Figure 35 SMARTech 5 - Air diffusion system for the nitritation, selection and accumulation SBR. .. 78 Figure 36 SMARTech 5 - Hydraulic testing ........................................................................................... 78 Figure 37 SMARTech 5 – Testing of the air diffusion system. ............................................................. 79 Figure 38 SMARTech 5 – Screenshot of the PLC control panel ........................................................... 79 EXECUTIVE SUMMARY Deliverable 3.2 is part of WP3 which is related to side- and down-stream SMARTechnologies. More specifically D3.2 focuses in three sidestream SMARTechnologies that are integrated in the existing conventional sewage sludge treatment line to provide more energy efficiency for the i) removal of SMART-Plant D3.2
Project: No 690323 nitrogen, ii) recovery of phosphorus and iii) recovery of PHA. The D3.2 is to the construction and the commissioning of the sidestream SMARTechs. A brief description of the sidestream Smartechs involved in WP3 is reported below: SMARTech 4a focuses in the integration of conventional biogas recovery from sewage sludge with sidestream energy-efficient and compact nitrogen removal and phosphorus recovery. It applies the Short-Cut Enhanced Nutrient Abatement system (SCENA) which integrates the following processes: (o) dynamic thickening of the mixed sludge, (i) acidogenic fermentation of cellulosic sludge to produce VFAs as carbon source, and (ii) via nitrite nitrogen and phosphorus removal (by P- bioaccumulation) from sludge reject water using an SBR. In this configuration, nitrogen is removed through the bioprocesses of nitritation/denitritation, and Enhanced Biological Phosphorus removal (EBPR) is accomplished via nitrite through the alternation of anaerobic/aerobic/anoxic conditions. SMARTech4b aims to the integration of the enhanced biogas recovery (by thermal hydrolysis) of sewage sludge with sidestream energy-efficient and compact nitrogen removal and phosphorus recovery. It applies and optimize the Short-Cut Enhanced Nutrient Abatement processfor the treatment of reject water with a very high ammonium nitrogen content (>1.2 gN/L) due to the pre- treatment of sewage sludge through thermal hydrolysis. In order to increase the biodegradable COD/N and COD/P ratios reject water from primary sludge gravity thickeners will be used. Alternatively, sodium acetate will be also employed to increase the readily biodegradable COD in reject water in order to efficiently remove nitrogen through short-cut nitrification/denitrification and to accumulate phosphorus in sludge through enhanced biological P removal via denitritation or aerobically. SMARTech4b is designed to treat approximately 2-3 m3/d of reject water from sludge dewatering facilities. Based on the design, alternative operational conditions can be employed depending on the type of external substrate provided. An SBR with an effective volume of at least 9 m3 will be installed and be equipped with aeration system, mixing apparatus, probes and meters for automatic control of the process. The SBR will be fed with sludge liquors form the dewatering unit and from primary sludge thickening unit. The sludge liquors before being fed to the SBR will be collected in two storage tanks. Three chemical dosing units will also be installed in order to provide SMART-Plant D3.2
Project: No 690323 i) for sodium acetate addition (as a complementary external substrate), and ii) for pH control of the process. SMARTech5 enables the integration of conventional biogas recovery from sewage sludge with the energy-efficient nitrogen removal from sludge reject water and the recovery of PHA and struvite. It applies the Short-Cut Enhanced Phosphorus and PHA Recovery concept (SCEPPHAR), which was conceived as a modified version of SCENA for WWTPs larger than 150 kPE. It accounts of the following sub-processes: (i) acidogenic fermentation of cellulosic primary sludge for the production of VFAs and the release of nitrogen and phosphorus in soluble forms (ammonia and phosphate); (ii) solid and liquid separation of the fermentation products and recovery of struvite form the sewage sludge fermentation liquid by the addition of Mg(OH)2 to favour phosphorus precipitation; (iii) ammonium conversion to nitrite accomplished in a SBR; (iv) selection of PHA storing biomass in a SBR by the alternation of aerobic feast conditions and followed by anoxic famine conditions for denitritation driven by internally stored PHA as carbon source; (v) PHA accumulation using a fed-batch reactor to maximize the cellular PHA content of the biomass harvested from the selection stage. SMART-Plant has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No 690323. SMART-Plant D3.2
Project: No 690323 ABBREVIATIONS AOB Ammonia Oxidizing Bacteria BNR Biological nutrient removal BOD5 Biochemical oxygen demand CHP Combined heat and power COD Chemical oxygen demand DO Dissolved oxygen DS Dissolved solids EBPR Enhanced Biological Phosphorus removal GHG Green house gases MLSS Mixed liquor suspended solids MLVSS Mixed liquor volatile suspended solids NH4-N Ammonium nitrogen NLR Nitrogen loading rate NOB Nitrite Oxidizing Bacteria ORP Oxidation-reduction potential OTR Oxygen transfer rate PHA Polyhydroxyalkanoates PLC Programmable logic controller SBR Sequencing Batch Reactor SCENA Short-Cut Enhanced Nutrient Abatement process SCEPPHAR Short-Cut Enhanced Phosphorus and PHA Recovery concept SL-DS Sludge liquor-Dewatered sludge SMART-Plant D3.2
Project: No 690323 SL-PS Sludge liquor-Primary sludge SOTE Diffuser efficiency SOTR Standard oxygen transfer rate SRT SVI Sludge volume index TN Total nitrogen TP Total phosphorus ΤS Total solids TSS Total suspended solids VFAs Volatile fatty acids VSS Volatile suspended solids WAS Waste Activated Sludge WWTP Wastewater Treatment Plant SMART-Plant D3.2
Project: No 690323 1. INTRODUCTION Deliverable 3.2 is part of WP3. WP3 main objective is to test and validate both side- and downstream SMARTechnologies. More specifically WP3 includes 1) three Sidestream SMARTechs that will integrate the existing conventional and enhanced biogas recovery from sewage sludge aiming at the energy-efficient removal of nitrogen, recovery of phosphorus and PHA and 2) two Downstream SMARTechs that will process the resource rich sludge to recycle raw material for following reuse in agricultural and construction sectors. WP3 consists of five tasks: Task 3.1 enabling sidestream SMARTech 4a with a duration of 42 months Task 3.2 enabling sidestream SMARTech 4b with a duration of 42 months Task 3.3 enabling sidestream SMARTech 5 with a duration of 42 months Task 3.4 enabling downstream SMARTech A with a duration of 30 months Task 3.5 enabling downstream SMARTech B with a duration of 30 months In the context of WP3 six deliverables are foreseen. Deliverables 3.1-3.3 & 3.5 are related to the three sidestream SMARTechs. The short title of each of the deliverables and their month of delivery is illustrated in Figure 1. Figure 1 Deliverables of WP3 related to sidestream SMARTechs. The present report is the second of these series of deliverables. D3.2 presents the costruction, installation and commissioning of the sidestream Smartetech. SMART-Plant D3.2
Project: No 690323 D3.2 is structured in four chapters and annexes, including this introduction, which presents the objectives of this report and its structure. For each technology, the report is structurized a technical of the SMARTech is 1- Technical description of the SMARTech 4a, 4b and 5; 2- List of the electromechanical equipment 4a, 4b and 5; 3- Practical instructions for the operation of SMARTech 4a, 4b and 5; 4- Drawings ‘as built’ 5- Picture reports Finally, Annex presents the executive drawing “as built” of the three Smartechs. SMART-Plant D3.2
Project: No 690323 2. SMARTECH4A - SIDESTREAM SCENA 2.1 Technical description of the SMARTech 4A The Smartech 4a is an innovantive technology aiming the via-nitrite nitrogen phosphorus removal from the anaerobic supernatant. The overall system can be described according to the following integrated operational units: 1) (alkaline) fermentation of thickened sewage sludge at mesophilic conditions (37°C) for the on-site production of best available carbon source (BACS), which is the optimal mix of volatile fatty acids; 2) A solid/liquid separation of the fermented sewage sludge by a screw press; 3) A Sequencing Batch Reactor (SBR) for the short cut biological nitrogen removal and phosphorus recovery via-nitrite through the dosage of the sewage sludge fermentation liquid. Figure 2 P&id of the Smartech 4a The optimization of the Smatech 4a was carried out during the design phase by the implementation of the dynamic thickening of the mixed sewage sludge, which allows the increase of the organic loading rate and the reduction of the sludge volume fed to the anaerobic digestor and the fermentation unit. The dynamic thickener (SCAE) allows the thickening of up to 100 m3 of sewage SMART-Plant D3.2
Project: No 690323 sludge per day, according with a flowrate of 20 m3/h. The final concentration of the sewage sludge will be around 5% (Total Solid based) thanks to the addition of a polyelectrolyte solution (0.8% of active compound) by a dedicated machine. Around 10 m3 of thickened sludge fed the fermentation unit, which has a total volume of 50 m3. The fermentation process works at around 30°C thanks to the heater fed to the biogas produced from the full scale anaerobic digestor. A constant hydraulic retention time of 5 days is controlled by two pneumatic and opposite valves, which are able to divert the flowrate of the thickened sewage sludge to the fermentation unit or to the digestor according with set-point level achieve in the fermentation unit. The solid/liquid separation of the fermented sewage sludge is carried out by a screw-press (SCAE) able to produce around 2-4 m3/h of fermentation liquid rich of volatile fatty acids. The liquid fractio is stored in a storage tank of 20 m3 to make it available for the further utilization during the anaerobic and anoxic phase of the scSBR. The solid fermented fraction (13-15% total solids based) is not disposed due to the still high biogas production potential, but it is mixed with the thickened mixed sludge which fed the anaerobic digestor. The scSBR has a maximal working volume of 70 m3, which allow the treatment of the daily flowrate of anaerobic supernant produced after the dewatering operation of the anaerobic digestate under 3-4 cycles. The scSBR is equipped with a mixing system having a nominal power of 1.5 kW. The aeration system consist of a volumetric blower (nominal power 11 kw) and n°80 diffusers (INVENT) able to provide around 500 m3/h of compressed air at 400 mbar of pressure, in order to provide an oxygen transfer efficiency up to 15%. The dissolved oxygen concentration in the bulk will be controlled during the aerobic phase at 1.5 mg/L by a Variable Frequency Device (VFD) to module the air flowrate of the blower. There are two centrifugal pumps from FLYGHT manufacturer with capacity of 70 and 65 m3/h respectively for the feeding and discharge of the scSBR. In each cycle, the feeding pump feeds automatically around 10-15 m3 of anaerobic supernatant, which is taken directly from the storage tank of 90 m3. The latter has a capacity to store enough anaerobic supernant for 2-2.5 days, which takes into account the days when the WWTP of Carbonera is not supervised from the operators (week-end) or when the dewatering operation are not taking placed. At the end of the cycle, the SMART-Plant D3.2
Project: No 690323 centrifugal sumberged pump installed at 0.8 m from the bottom of the scSBR allows the discharge of the treated anaerobic supernatant in the headworks of the main WWTP. The SBR is equipped with sensors from HACH-LANGE company which are based on a floating chamber. The sensors allows the monitoring of several parameters and by them also the control of the nitrogen forms, so to control the cycle lenght. The sensors installed are: pH, Dissolved Oxygen (DO), Conductivity (COND), Oxydation Reduction Potential (ORP), Mixed Liquor Suspended Solids (MLSS). All the signal from the sensor are first collected by the controller SC1000 (HACH-LANGE) and then transfer to a Programmable Logic Controller (PLC, SIEMENS) via a modbus protocol. The data can be also recorded and used from the remote system of ATS. The control algortims installed in the PLC provides the control of the electrical equipments, including the lenght of each phases, the automatic dosage of the carbon source and the variable frequency driver to control the right dissolved oxygen during aerobic phase. SMART-Plant D3.2
Project: No 690323 2.2 List of the electromechanical equipment Table 1 Specification of the grinder for the mixed primary sludge. GRINDER CODE DESCRIPTION Unit Value TR1 Grinder m3/h 20 rpm 270 Hz 50 Description The grinder is used as for the size reduction of the coarse material present in the mixed sludge. The grinder has 4 self-sharpening cutting blades with a grid having a maximal pore size of 24 mm and 445 cm2 of surface. The maximal operating pressure is 2 bar. Table 2 Specification for the installation of the dynamic thickening DYNAMIC THICKENING CODE DESCRIPTION Unit Flowrate ID Dynamic thickening m3/h 20 List of electromechanical equipment included CODE DESCRIPTION Flowrate Intalled CONTROL power P4 Feeding ID 20 m3/h 7.5 P7 Emulsion dosage 0-600 L/h - P8 Poly solution dosage 2 m3/h 1.1 P16 Washing ID pump 3 5 m /h 5.5 P05 Feeding DA, POI, FRM 3 6 m /h 4 FLOW Feeding from (F)/ Discharge to (D) PUMP CODE Configuration 1: PRI -> ID -> FRM; F1:P04 Configuration 2: PRI -> ID -> POI; F2:P07, P08 Configuration 3: PRO ->ID-> DA D1: P05 D2: gravity SENSORS INSTALLED Code M012 Description Measurement of the total solids of the mixed sludge Technical description Probe with combined light infrared absorption for measuring turbidity and suspended solids Independent of the color of the water sample (suitable for waste activated sludge, primary sludge, SMART-Plant D3.2
Project: No 690323 etc). Component and configuration Configuration: insertion probe with steel probe body; Lenght of cable: 10 meters Technical data: photometer with double IR detector Method of measurement: Turbidity measurement according to DIN EN 27027; Measure Solids, equivalent to DIN 38414 Measurement range: Turbidity: 0.001 - 4.000; Total Solids: 0.001 - 50.0 g / l Accuracy: 1.0% turbidity, ± 0.001 FNU Coeff. Var process: 1.0% according to DIN 38402 Response Time: 0.5 s
Project: No 690323 Table 3 Specification of the fermentation unit FERMENTATION UNIT CODE DESCRIPTION Size Value FRM Fermentation unit Diamete 4m Height 4m List of electromechanical equipment included CODE DESCRIPTION Flowrate Intalled CONTROL power P05 Feeding FRM 3 6 m /h 7.5 Based on status of V3 and V4 P09 Discharge FRM 3 6 m /h 0.55 MX5 Mixer FRM - 1.5 Manual switch on/off HH Heater 55 (daily 14.7 kW The biogas is taken from the needs of thermic full scale anerobic digestion of biogas) power sewage sludge FLOW Feeding from (F)/ Discharge to (D) PUMP CODE FRM -> PC F1:P05 D1:P09 SENSORS INSTALLED Code M010 Description Measurement oft he pH and temperature of the fermentation unit (FRM) Technical description Differential type digital sensor for the measurement of pH and temperature. Electrode not in contact with the liquid bulk. Component and configuration Material of the electrode: glass; Type of probe: submerged Sensor body: steel Range of measurement: 0 - 14; T=-5° C a 50° C Time of response: pH: < 5 s; T: < 2 min Reference electrode for the control of the impedence of the liquid bulk Lenght of the cable: 10 metri Dimensions: 350 x 44 mm (diameter) Other equipments included - Fixing system for pH, size 1" steel AISI316 SMART-Plant D3.2
Project: No 690323 Table 4 Specification for the installation of the screw-press separator for the mixed sludge fermentation SCREW PRESS SEPARATOR CODE DESCRIPTION Unit Flowrate PC Screw Press for sludge m3/h 2-4 fermentation dewatering List of electromechanical equip-ment included CODE DESCRIPTION Flowrate Intalled CONTROL power P09 Feeding DA, POI, FRM 3 6 m /h 4 Controlled by frequency inverted and leve ultrasonic P13 Poly solution dosage 0.32 Controlled by frequency inverted and leve ultrasonic P11 Solid 3 fraction 0.6-3.2 m /h 5.5 Controlled by frequency fermentation sludge inverted and leve ultrasonic P10 Liquid fraction 2-5 m3/h 1.4 Controlled by min/max level fermentation liquid sensor M022 FLOW Feeding from (F)/ Discharge to (D) PUMP CODE FRM-> PC -> SCENA (Liquid fractio) F1: P09; FRM ->PC -> POI (Solid fraction) F2: P13 D1: P11; D2: P10 POLYELECTROLITE MACHINE CODE DESCRIPTION Flowrate VALUE PP2 Machine for preparation of m3/h polyelectrolyte solution List of electromechanical equipment included CODE DESCRIPTION Flowrate Intalled CONTROL power P7 Emulsion dosage 0-600 L/h 0.5 P8 Poly solution dosage 1.1 FLOW Feeding from (F)/ Discharge to (D) PUMP CODE PP2 -> FRM F1: P7; PP2 -> ID D1: P8 D2: Table 5 Specification of the Short-Cut Sequencing Batch Reactor SMART-Plant D3.2
Project: No 690323 SHORT-CUT SEQUENCING BATCH REACTOR CODE DESCRIPTION Size Value scSBR Short-Cut Sequencing Batch Max working 70 m3 Reactor Volume Surface 8 x 2.9 m Height 3.2 m List of electromechanical equipment included CODE DESCRIPTION Flowrate Intalled CONTROL power P1 Feeding scSBR 3 49 m /h 1.8 Switch on during the filling phase (control by the PLC) MX3 Mixer scSBR - 1.5 Switch on during the filling, anaerobic and anoxic phase. (control by the PLC) BL1 Blower scSBR 3 170 ÷ 520 m /h 11 Switch on aerobic phase. (control by the PLC) P2 Discharge scSBR 70 m3/h 1.35 Switch on during the discharge phase (control by the PLC) P12 Carbon source 3 5 m /h 0.98 Switch on during the anaerobic and anoxic phase (control by the PLC) P03 Purge 3 5 m /h 2.2 Manual switch on/off FLOW Feeding from (F)/ Discharge to (D) PUMP CODE FRM -> PC F1:P05 D1:P09 INSTALLED SENSORS Code DO002 Description Measurement of dissolved oxygen of the selection SBR unit (R006) Technical description The measurement method is based on the emission of luminescent radiation by a special substance (luminophore) that is excited by light blue emitted by a LED and returning to the normal state emits light red. A photodiode measures the time needed to return to the quiescent state, inversely proportional to the concentration of oxygen present on the luminophore. Component and configuration - Measuring principle: luminescent optic - Measurement range: 0 to 20.00 mg / L (ppm) O2, 0 to 200% saturation - Accuracy: 0-5 mg / L O2 ± 0.1 mg / L, 5-20 mg / L O2 ± 0.2 mg / L; Temperature: ± 0.2 ° C - Repeatability: ± 0.1mg / L - Resolution: 0.01 mg / L (ppm) O2 / 0.1% saturation SMART-Plant D3.2
Project: No 690323 - Response time (at 20 ° C): T90
Project: No 690323 - PVC pole (Ø 40mm, length 2 meters) - 1 "NPT sensor adapter - swivel spindle - brown tube closure cap SMART-Plant D3.2
Project: No 690323 2.3 Practical instructions for the operation of SMARTech 4A The dynamic thinkening is fed using the volumetric pump P04 with a flow rate of 20 m3/h. To prevent clogging due to tatters or other inert materials, a grinder by vogelsang company is installed before the pump P04. However, in case of mantenance or techical problems, the P04 can be replaced by the parent installed volumetric pump P06. The thickened mixed sludge (50 gTSS/L) is pumped using a volumetric pump at 6 m3/h. The influent flowrate and the total solid concentration of the influent mixed sluge are monitored by the inline sensors M012 (TSS) and M014 (Qf) respectively. A solution of polyelectrolite is provided using the volumetric pump P09, where the flowrate is automatically adjusted according with the registered total solids concentration of the influent and thickened mixed sludge using the inline sensors M013 (TSS) and M015 (Qdig) respectively. Every day, 10 m3/d of fermented sludge are discharge from the fermentation unit using the P09 and then fed with fresh 10 m3/d of thickened mixed sludge using the P05. The feeding and discharge of the fermentation unit are controlled by the level sensor M009 and based on two opposite pneumatic valves (V3 and V4). At minimun fixed level, the pneumatic valve V4 is kept closed, while the pneumatic valve V3 is open, so to allow the feeding of thickened. The duration of the feeding is 1.7 hours. Once the maximal level of the fermentation unit is achieved, the valve V3 close and V4 open. Table 6 Operation of the fermentation unit Operation phase Parameter that defines the phase Equipment in working duration according to PLC design mode during this phase controlled by PLC Filling (1 per day) Level max The valve V3 open while the valve V4 is closed Decanting (1 per day) Level min The valve V4 open while the valve V3 is closed The screw press is fed using a volumetric pump with a maximal flowrate of 2-4 m3/h. The solid and liquid separation of the mixed sludge fermentation results on two main stream: solid and liquid. The liquid is pumped by a centrifugal pump using the storage tank of the carbon source. The solids fraction is pumped by to the post dynamic thickening using the volumetric pump P11. The P9 is controlled by the level of the fermentation. Every day, the screw press accomplishes the solid/liquid SMART-Plant D3.2
Project: No 690323 separation until when the minimun level of the fermentation unit is achieved. The fermentation liquid produced is relaunched by the pump P10 from a temporary tank to the final storage tank of 20 m3 for its further application to the scSBR. The P10 is turned on when the level of the carbon source is between the minimun and maximal level of the M022. The P10 stops the operation as soon as the maximal level M011 is achieved. The eventual excess of carbon source production is drained by the overflow and so discharged in the mainstream. Table 7 Operation of the screw-press separator Operation phase Parameter that defines the Equipment in working mode phase duration according to PLC during this phase controlled by design PLC Filling Operation according to the level P9 MIN and MAX of the fermentation unit Relunch of the liquid Operation according to M022 P10 fraction Discharge solid fraction Operation according to M011 P11 The scSBR is fed with around 40 m3/d of anaerobic supernatant using the suberged centrifugal pump P01. The carbon source is provided by the volumetric pump P12. The effluent from the scSBR is discharged using the submerged centrifugal pump P02. The waste activated sludge is withdrawn from the scSBR using the P03. The anaerobic supernatant from the dewatering operation of the digestate is sent by gravity in the equalization tank. The level M001 controlled the operation of two pneumatic valve V13 and V14: at the minimal level achieved, the V13 is closed and V14 is opened, while at the maximal level achieved the V13 is opened and V14 is closed. The daily flowrate of anaerobic supernatant provided to the scSBR is divided in three or four cycle. The level M002 determines the minimal and the maximal level achievable in the scSBR. Six sensors are installed in the reactor: conductivity (M003), pH (M004), ORP (M005), DO (M006), MLSS (M007) and N2O (M008). Among them, DO is used to control the compressor through VDF, while conductivity and pH are used to control the lenght of the aerobic phase, the amount of carbon source and the lenght of the anoxic phase. The other sensors are not included in the control algorithm of the system but are recorded in the PLC. SMART-Plant D3.2
Project: No 690323 Table 8 Operation of the short-cut Sequencing Batch Reactor. Operation phase Parameter that defines the phase Equipment in working duration according to PLC design mode during this phase controlled by PLC Filling Timer or/and Level meter SBR mixing device Sludge liquors feeding pumps Anaerobic phase Time based control SBR mixing device (1 phase for each cycle) Monitoring of the process parameters (pH, ORP, Conductivity, Oxygen, N2O, MLSS) Aerobic phase Time based controlled for the Min Frequency of the blower (1-2 phases during each and Max lenght of the phase; control by a PID algoritm cycle) Real time control based on conductivity and pH Anoxic phase Time based controlled for the Min SBR mixing device; (1-2 phases during each and Max lenght phases Carbon source feeding; cycle) Dosage of the carbon source according with the conductivity; End of the phase according with pH signals Settling Timer - Decanting Timer or/and Level meter Disharge pump WAS removal Timer or/and Level meter Decanting pump SBR mixing device 2.1 Integrability of the Smartech 4a in existing WWTPs Integrability issues Smartech 4a Technical Feasibiliy 1. Should new facilities always be No. Preliminary designs should be always performed in considered during the design and order to consider the recovery of disused tanks or the implementation of the Smartech? conversion of the existing facilities in the WWTPs. In particular, the Smartech 4a was designed considering SMART-Plant D3.2
Project: No 690323 the conversion of existing tanks dedicated to the storage of liquid waste. 2. Does the implementation of the No, if the Smartech 4a takes advantage of existing Smartech imply a substantial change of works, only minor changes of piping connection are the present flowscheme of the WWTP? required, which do not represent substantial changes of the WWTPs. 3. Could the Smartech negatively impact No, the Smartech will positively impact on the final on the final discharge of the main discharge, because the treated effluent from Smartech WWTP? 4a is supposed to contain up to 90% less nitrogen and 30-60% less phosphorous compared with raw anaerobic supernatant. However, even if the technology does not perform as expected, the effluent will be treated in the main WWTPs before its final discharge in the water body. Acceptability of the Smartech 1. Is the Smartech 4a well accepted The Smartech 4a is considered by operators an among the operators? integrated and useful compartment of the WWTP and the personnelle are used to operate and take care of it. 2. Are specific skills and/or tranings No additional specific trainings are requireds. The required for the operators? knowledge and expertize already held by the operators of the main WWTP are also sufficient and adequate to operate in the Smartech 4a. The latter in fact uses the same equipments typically adopted also by conventional biological processes. SMART-Plant D3.2
Project: No 690323 Bureaucratic issues 1. Did Smartech 4a require a specific Yes. The authorization for its implementation was authorization for its implementation? asked to the Regional Authority (see the attachment). Are there any standards, regulations or No, the Smartech 4a does not need to conform to references applicable? specific regulation. However, if new facilities are implemented, the competent autority may ask to respect the standards of the “landscaping regulation”. However, regulations could significantly change based on the country where the plant is operating. 2.2 Drawings ‘as built’ The drawings of the units are reported in the following annexes: • Drawing 1: P&id of the Smartech 4a • Drawing 2: Fermentation unit • • Drawing 3: Layout of the Smartech 4a • Drawing 4: Dynamic Thickening • Drawing 5: Screw press separator SMART-Plant D3.2
Project: No 690323 2.3 Picture report Figure 3 SMARTech 4a - Dynamic thickener of the sewage sludge Figure 4 SMARTech 4a – Screw-press for S/L of the fermentation sewage sludge SMART-Plant D3.2
Project: No 690323 Figure 5 SMARTech 4a – Accumulation tank for the fermentation liquid of mixed sludge Figure 6 SMARTech 4a – Different views of the fermentation SMART-Plant D3.2
Project: No 690323 Figure 7 SMARTech 4a - Electrical Panel and air compressor of Smartech 4a Figure 8 SMARTech 4a -Tank for the acculation of the anaerobic supernatant and influent pump of the scSBR SMART-Plant D3.2
Project: No 690323 Figure 9 SMARTech 4a - Air diffusion system of the scSBR SMART-Plant D3.2
Project: No 690323 3. SMARTECH4B - SIDESTREAM THERMAL HYDROLYSIS-SCENA 3.1 Technical description of the SMARTech 4B The SMARTech 4b pilot system is an innovative nutrient removal process via nitrite which is integrated in the Psyttalia WWTP in order to manage the reject water produced from the dewatering process of the plant. The SMARTech 4b shall treat separately the reject water of the dewatering process to biologically remove nitrogen and phosphorus and then recycle it back to the inlet of the WWTP (Figure 3.1). This process also takes advantage of the readily biodegradable COD which is contained in the reject water of the primary thickened sludge in order to provide part of the carbon source which is required to remove nutrients from dewatered sludge. Figure 10 Flow diagram of Psittalia WWTP with SMARTech 4b Figure 10 illustrates the major units of the pilot system along with their interconnections. The core of SMARTech 4B is the bioreactor (SBR). The SBR is a rectangular tank with dimensions [2.00x2.30x2.40] [WxLxH] and 9m3 maximum active volume. The construction material is stainless steel AISI 304L. SMART-Plant D3.2
Project: No 690323 Figure 11 Major units of SMARTech 4b and their interconnections The SBR is equipped with a mixing apparatus in order to provide a minimum mixing capacity of 8 W/m3. The mixer manufacturer is SEKO (Italy) and it is a slow speed 200rpm mixer with 220mm propeller, stainless steel shaft and PVC body. The effective depth of the reactor will be at least 1.5 m (during the aeration phases) in order to allow for an oxygen transfer efficiency to the order of 8-10%. An aeration system with diffusers has been installed in order to meet the oxygen requirements of the system. The aeration system consists of a side channel air compressor from MAPRO International with maximum capacity of 252 m 3/h at 200 mbar and fine bubble AEROSTRIP diffusers Type T provided by Aquaconsult. The transfer efficiency of the diffusers is in the order of 100 m3/m2 h. The SBR will be fed with sludge liquors from the dewatering unit and from the primary sludge thickening unit. The sludge liquors upstream the SBR will be collected in two storage tanks (one for each type of sludge liquors). There are two transfer pumps from NETZSCH manufacturer with capacity of 5 m3/h each, which feed the storage tanks in automatic mode, in order to keep the necessary volume of slugde liquors in the storage tanks. Each tank provides a storage capacity of min 2 d, with an effective volume to the order of 8 m3 each. Both storage tanks are made of polyethylene, black color, with roof manhole. Each of these storage tanks is equipped with a submersible centrifugal pump (two in total) from LOWARA manufacturer for continuous mixing of the content. Each type of sludge liquors will be fed into the SBR with the use of an eccentric screw pump. The installed feeding pump is from NETZSCH manufacturer and it is driven by VFD (frequency converter). SMART-Plant D3.2
Project: No 690323 The maximum capacity of the pump is 7 m3/h. The selection of the capacity of this pump is based on: i) the maximum daily flow rate of the sludge liquors (3 m3/d for the SL-DS and 2.65 m3/d for the SL- PS), ii) the minimum number of 3 cycles per day and iii) the duration of fill phase of 15 min. A second eccentric screw pump, from NETZSCH manufacturer and also driven by VFD has been installed in order to provide decanting of treated sludge liquors from the SBR and the removal of the surplus activated sludge as well. The waste activated sludge will be collected temporarily in a rectangular storage tank made of polyethylene and of volume 1m3, which is sufficient for 2 days storage of sludge removed. A solution of acetic acid (in the form of sodium acetate) will be added to the reactor to meet the biodegradable organic carbon requirements. The external organic carbon system consists of a storage tank with an active volume of 1 m3 and it is sufficient for more than 7 days storage capacity. The tank is made of polyethylene and it is placed in an appropriate leakage basin. It is equipped with a mixer from SEKO manufacturer. A dedicated diaphragm, adjustable flow-rate dosing pump from DOSEEURO AP manufacturer with a capacity of 200 L/h is installed in order to transfer the sodium acetate solution from the storage tank to SBR. It is expected that under normal conditions there will not be any need for pH control for the pilot system. However, as the performance of especially the nitritation – denitritation processes is highly dependent on the pH and the fact that under transient conditions (especially during start-up) there might be a need for pH control, a pH control system has been installed in the pilot system. The pH control system consists of an acid dosing system and a base dosing system. The acid (in the form of sulfuric acid) dosing system consists of a storage tank with a volume of 1 m3 and a diaphragm, adjustable flow-rate dosing pump from DOSEEURO AP manufacturer with a capacity of 50 L/h. A separate similar dosing system is provided for the addition of the base (in the form of sodium hydroxide). Both chemicals storage tanks are placed in a leakage basin. The SBR is equipped with a piezoelectric level transmitter from ENDRESS+HAUSER company and several analytical field instruments such as pH, ORP, DO, Temperature, Conductivity, NH4-N, NO2- N/NOx-N from the WTW company. All the instrumentation will be collected in a common controller SMART-Plant D3.2
Project: No 690323 WTW MIQ, which will be interconnected with PLC via Profibus DP interface. All the storage tanks will be equipped with suitable level switches. All electrical and automation equipment, including motor starters, variable frequency drives and PLC, have been installed into a stainless steel IP55 enclosure (2000x600x600mm) from SABO manufacturer, forming the Motor Control Center (MCC) of the pilot plant system. The electric power supply is at 400VAC/3–phase and the control voltage at 24VDC. The process automation (e.g. feeding, aeration, decanting, was, chemical dosing) will be carried out in automatic mode by the CPU PLC but there is also an HMI device (touch panel) for controlling the equipment manually and monitoring all measured values from instrumentation locally. Finally, the MCC will be ready for interconnection to an external PC for data acquisition. 3.2 List of the electromechanical equipment The technical specifications of the major units and the electro-mechanical equipment installed at the site are presented in Table 3.1. SMART-Plant D3.2
Project: No 690323 Table 9 Major units and specifications of the electro-mechanical equipment SMART-Plant D3.2 Page 36
Project: No 690323 SMART-Plant D3.2 Page 37
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Project: No 690323 3.3 Practical instructions for the operation of SMARTech 4B The operation of SMARTech 4B includes a series of actions and settings which can be divided in the following categories: • Preparation of chemicals to be dosed in the reactor • Selection of the automation mode and definition of the set points • Calibration of on-line probes Preparation of chemicals Three types of chemicals will be used during the operation of SMARTech 4B: the substrate, the acid and the base for pH control. Among these the acid-base chemicals will be supplied as ready to use solutions with the already specificed characteristics and therefore no specific actions will be needed from the operators of the system. The only care will be to send a notice for refill the chemicals tanks upon signal of low level. Substrate as sodium acetate will be dosed to the reactor automatically. The preparation of the solution in the respective tank will be undertaken by the operator of the system. The solution wiil be prepared by adding sodium acetate powder to the tank in order to reach an acetic acid content of 200 kg/m3. Selection of automation mode SMARTech 4b is equipped with online monitoring meters and a programmable logic controller (PLC) which will provide operational flexibility and applicability of different control strategies. Online probes of dissolved oxygen, pH, temperature, conductivity, oxidation-reduction potential, NH4-N, NOx and a level meter have been installed into the surface of SBR unit and real time information on the performance of the system will be obtained and transferred to the online controller every 1 minute. The PLC is interconnected to an external PC for data acquisition. SMART-Plant D3.2 Page 39
Project: No 690323 All the major units of the electro-mechanical equipment such as the SBR mixer apparatus and the mixing devices of storage tanks, feeding, dosing and decanting pumps and the air blower are connected to the PLC which control their operation according to predefined parameters or schedule. The main operational strategy that will be established is based on time schedule and online sensors measurements. More specifically, every SBR cycle has a number of distinct phases. For each phase a variety of functions and processes have been programmed under the regulations of the PLC according to the automation plan. Table 10 describes the basic features of the automation to control the operation pf the system. Table 10 Basic features of automation in the operation of pilot plant system. Operation phase Parameter that defines the Equipment in working mode phase duration according to PLC during this phase controlled by design PLC Filling Timer or/and Level meter SBR mixing device Sludge liquors feeding pumps Anaerobic phase Timer SBR mixing device (1-2 phases during each pH adjustment system cycle) acid/base dosing pumps Aerobic phase Main operation: Timer or/and Air blower (1-3 phases during each NH4-N sensor measurements pH adjustment system cycle) Alternativelly: pH set point or pH acid/base dosing pumps slope Control of blower flow rate Anoxic phase Main operation: Timer or/and SBR mixing device (1-3 phases during each NOx sensor measurements Substrate feeding pumps cycle) Alternativelly: ORP slope or pH pH adjustment system set point or pH slope acid/base dosing pumps Settling Timer - SMART-Plant D3.2 Page 40
Project: No 690323 Decanting Selected valve of decanding Decanting pump pump SAS removal Selected valve of decanting pump Decanting pump SBR mixing device Based on the design of the automation system the operator is able to choose the number of each phase (e.g. anaerobic, anoxic, aerobic) during each cycle as well as their sequence. The maximum number of process functions/phases that can be selected in each cycle is eight (two anaerobic, three anoxic and three aerobic). Filling phase is starting upon setting the feeding pump on. The duration of the feeding phase is primarily based on the set point of the level meter. For safety reasons the maximum duration of this phase can also be regulated by a timer. The duration of the anaerobic phase is primarily regulated by a timer. During this phase, the PLC will set up the SBR mixing system and if necessary will control the pH adjustment system providing acid or base solution from the storage tanks using two dosing pumps. It is expected that under transient conditions and especially during start-up there will be a need for pH control to the desired set points by providing sulfuric acid or sodium hydroxide. During the aerobic phase the PLC will activate the aeration system while the mixing system will ceased operation as adequate mixing will be provided by the diffusers. The air flow rate provided by the blower will be regulated according to the desired set point of dissolved oxygen in the reactor. The duration of the aerated period will be controlled either by a timer or by a critical value of NH4-N sensor (or both). The automation system provides also alternative control functions of the duration of this phase based either on the pH set point or on pH slope. During the aerated phases pH control can be impleened (if desired) by regulating the acid/base dosing system. Following the aerobic phase, the anoxic phase will start with the end of aeration and the addition of external carbon source (fiilling). In order to meet the biodegradable organic carbon requirements for denitritation procces the automation system will be set to provide adequate volumes of primary SMART-Plant D3.2 Page 41
Project: No 690323 sludge liquor or acetate or a mix of the two substrates. A maximum of three dinstict anoxic phases can be implemented during each cycle and their duration will be controlled by either a timer or by reaching a pre-defined value of NOx sensor (or both). Furthermore, alternative control strategies can also be choosen by the operator based on set points defined for ORP, pH and pH slope. During each anoxic phase the PLC will maintain open the mixing system and will also provide pH control. The surplus activated sludge (SAS) removal will take place either during aerobic or during anoxic phase in the form of mixed liquor in order to keep the desried sludge age. After the last anoxic period in each cycle, the PLC will stop the mixing system and sedimentation phase will take place for a pre-selected time period. Every cycle will end up with decanting. The PLC will control the volume of supernatant that the decanting pump will remove from the SBR unit either by a timer or by the level meter measurements. In view of the above, the operator selects the mode of automation and specifies the set points directly on the screen pf PLC. Calibration of on-line probes Calibration of the on-line probes will take place on a weekly basis. In this context the operator will collect activated sludge samples which will be analyzed for pH, conductivity, ORP, NH4-N, NO2-N, NOx- N and the results will be compared with the on-line measurements for validation. Upon significant deviations calibration of the on-line probes will take place. 3.1 Integrability of the Smartech 4b in existing WWTPs Integrability issues Smartech 4b Technical Feasibility SMART-Plant D3.2 Page 42
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