Dynamic Testing of Lime-Tree (Tilia Europoea) and Pine (Pinaceae) for Wood Model Identification - MDPI
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materials Article Dynamic Testing of Lime-Tree (Tilia Europoea) and Pine (Pinaceae) for Wood Model Identification Anatoly Bragov 1 , Leonid Igumnov 1,2, *, Francesco dell’Isola 1 , Alexander Konstantinov 1,2 , Andrey Lomunov 1 and Tatiana Iuzhina 1 1 Research Institute for Mechanics, National Research Lobachevsky State University of Nizhny Novgorod, 603950 Nizhny Novgorod, Russia; bragov@mech.unn.ru (A.B.); fdellisola@gmail.com (F.d.); constantinov.al@yandex.ru (A.K.); lomunov@mech.unn.ru (A.L.); yuzhina_tatiana@mech.unn.ru (T.I.) 2 Research and Education Mathematical Center “Mathematics for Future Technologies”, 603950 Nizhny Novgorod, Russia * Correspondence: igumnov@mech.unn.ru; Tel.: +7-910-792-7826 Received: 22 October 2020; Accepted: 19 November 2020; Published: 20 November 2020 Abstract: The paper presents the results of dynamic testing of two wood species: lime-tree (Tilia europoea) and pine (Pinaceae). The dynamic compressive tests were carried out using the traditional Kolsky method in compression tests. The Kolsky method was modified for testing the specimen in a rigid limiting holder. In the first case, stress–strain diagrams for uniaxial stress state were obtained, while in the second, for uniaxial deformation. To create the load a gas gun was used. According to the results of the experiments, dynamic stress–strain diagrams were obtained. The limiting strength and deformation characteristics were determined. The fracture energy of lime and pine depending on the type of test was also obtained. The strain rates and stress growth rates were determined. The influence of the cutting angle of the specimens relative to the grain was noted. Based on the results obtained, the necessary parameters of the wood model were determined and their adequacy was assessed by using a special verification experiment. Keywords: timber; natural composite; Kolsky method; deformation diagrams; wood species; energy absorption; wood model; verification 1. Introduction Wood is a complex natural composite. It is widely used as a material for damping intensive dynamic loads of shock or explosive nature. In order to conduct reliable numerical analysis of the designs of containers for transporting hazardous substances, using wood as shock damping components, reliable mathematical models are required that take into account its complex multicomponent structure of wood. The actively developing models of wood deformation and destruction can be used in various design complexes to simulate the behavior of technically complex structures that incorporate wood elements. However, the complex nature of wood means that not a single model can be used for all purposes, thus different models must be used to solve various specific problems. In order to reliably describe the behavior of wood in a dynamically loaded structure, its model should include a sufficiently large set of parameters that take into account the deformation anisotropy and the dependence of the strength properties on the strain rate, density, temperature and moisture content. For example, in the manual for the LS-DYNA software package, the wood model No. 143 has 29 parameters: five modules for transversely isotropic constitutive equations, six tensile strengths for yield criteria, four hardening parameters to peak stresses, eight softening parameters after peak, and six parameters speed effect [1]. The LS-DYNA calculation complex library contains model parameters for only two wood species: southern yellow pine and Douglas fir. This necessitates detailed studies of various wood species Materials 2020, 13, 5261; doi:10.3390/ma13225261 www.mdpi.com/journal/materials
Materials 2020, 13, 5261 2 of 12 for various types of stress–strain states in a wide range of strain rates and temperatures, in order to equip mathematical models of wood with parameters (identification) that can adequately describe the behavior of the engineering structure containing wood components under shock wave loads. The first detailed review of using wood as an element of damping structures was given by Johnson [2]. In the report, he noted that the dynamic properties of wood are not well understood. In the past three decades, quite a lot of works have appeared that explored various aspects of the high-speed deformation and destruction of wood, including the use of wood as a damping material in containers for transportation of radioactive materials by air, road and rail transport [3]. A large amount of research into the dynamic properties of wood was performed by Reid et al. [4–6]. In these works, the dependences of destructive stress and energy absorption on the impact velocity were obtained. It was noted that dynamic destructive stresses are several times higher than static ones. The authors also postulated that failure stresses of specimens fabricated along the grain are an order of magnitude higher than that of the specimens cut transverse to the grain. The relationship between mechanical parameters of selected wood species (Carya sp., Fagus sylvatica L., Acer platanoides L., Fraxinus excelsior L., Ulmus minor Mill.) and the grain orientation angle concern loading direction was investigated in [7]. It was observed that as the angle between fibers and loading direction increases whereas the mechanical characteristics of all wood species decrease. In the works of Bragov et al., using the Kolsky method, dynamic diagrams of birch, aspen, and sequoia were obtained at strain rates of ~103 s−1 with different direction of cutting specimens relative to the direction of timber fibers [8,9]. The deformation diagrams of specimens under loading along the grain are much higher than those under loading transverse to the grain. The limiting deformative characteristics have the opposite direction. In recent years, interest in studying the effect of moisture, density and cutting angle on the mechanical properties of wood has increased significantly. Adalian et al. [10] and Eisenacher et al. [11] carried out a cycle of tests on wood in the range of strain rate from 10−3 to 103 s−1 . Wouts et al. [12], Ha et al. [13,14] and Hao et al. [15] considered the damping ability of various biological materials of plant origin from the point of view of improving artificial damping structures. Mach et al. [16] calculated the hysteresis losses (dissipated energy) as the area bounded by the loading and unloading curves, whereas stored energy (recoverable energy) is defined as the area under the unloading curve. Thus, the total energy is calculated by summing the area of the hysteresis loss and the stored energy. In the work of Novikov et al. [17], a large number of tests of sequoia, birch, aspen, and pine was carried out at different cutting angles, temperatures ranged from −30 ◦ C to +65 ◦ C, and at the moisture content of 5%, 20% and 30%. As a result, the dependence of strength on moisture and cutting angle was determined. The mechanical properties of wood strongly depend on the place of growth, its age, the place of cutting and the type of stress–strain state. Therefore, the results obtained by different authors may differ significantly from each other. The purpose of this work is to conduct a detailed study of the effect of strain rate and type of stress–strain state on the mechanical properties of wood as well as to identify and verify the wood model. 2. Test Methods, Materials and Specimens For dynamic compressive tests of wood, the Kolsky method and split Hopkinson pressure bar (SHPB) technology were used [18]. Figure 1 shows the installation diagram, as well as the main formulas for determining the parametric dependencies of deformation, stress and strain rate of the sample under compression. Two measuring bars were made of high-strength aluminum alloy and had a diameter of 20 mm and length of 1.5 m. During testing, a striker accelerated in the barrel of a gas gun impacts the SHPB and excites an elastic compression wave in the loading measuring bar, which, upon reaching the specimen, deforms it. The second (support) measuring bar acts as a dynamometer-waveguide and allows you to register the transmitted strain pulse εT (t) and then to determine the process of stress developing in the specimen. The pulse εR (t) reflected from the specimen in the loading bar makes it
Materials 2020, 13, Materials 2020, 13, 5261 5261 33 of of 12 12 specimen, and its integration allows to determine the process of the specimen deformation possible to determine the process of strain rate change in the specimen, and its integration allows to development. Small-length foil strain gages were used for registration elastic strain pulses in the bars. determine the process of the specimen deformation development. Small-length foil strain gages were Based on these pulses, the parametric processes of stress, strain and strain rate over time are used for registration elastic strain pulses in the bars. Based on these pulses, the parametric processes of calculated using the formulae shown in the lower part of Figure 1. Then, excluding time as a stress, strain and strain rate over time are calculated using the formulae shown in the lower part of parameter, a dynamic stress–strain curve is constructed with the known law of variation of the strain Figure 1. Then, excluding time as a parameter, a dynamic stress–strain curve is constructed with the rate [19]. known law of variation of the strain rate [19]. Figure 1. Installation scheme and basic dependencies. Figure 1. Installation scheme and basic dependencies. Dynamic tests were carried out with specimens of lime-tree (Tilia europoea) and pine (Pinaceae) with aDynamic diametertests of 20were carried mm and out with a length of 10specimens mm, cut from of lime-tree solid wood(Tilia europoea) at an 0◦ and angle ofand pine ◦ relative 90(Pinaceae) with to theaaxis diameter of 20trunk. of the tree mm andThe aflat length ends of the 10 mm, cut from samples solid wood were carefully at an angle before hand-grinded of 0° and 90° testing. relative The to theparameters physical axis of the of tree trunk. tested The flatare materials ends of theinsamples shown were the Table 1. carefully hand-grinded before testing. The physical parameters of tested materials are shown in the Table 1. Table 1. The physical parameters of tested materials. Table 1. The physical parameters of tested materials. Wood Species Lime-Tree Pine Wood Species Parameter Along the GrainLime-Tree Transverse to the Grain Along the Grain Pine Transverse to the Grain Parameter 3 Along the Grain Transverse to the Grain Along the Grain Transverse to the Grain Density, g/cm 0.505 ± 0.02 0.512 ± 0.015 0.435 ± 0.01 0.484 ± 0.015 Density, g/cm3 0.505 ± 0.02 0.512 ± 0.015 0.435 ± 0.01 0.484 ± 0.015 Moisture content,%% Moisture content, 7.5 ± 0.2 7.5 ± 0.2 7.9±±0.3 7.9 0.3 6.8 ±± 0.3 6.8 0.3 7.1±± 0.2 7.1 0.2 The total The totalamount amountofoftested tested samples samples of of eacheach wood wood species species amounted amounted 50 pieces: 50 pieces: 40 pieces 40 pieces were were used used for for mechanical mechanical testing testing and 10and 10 pieces pieces were were used used for subsequent for subsequent woodwood model model verification. verification. In each In each test test mode during mechanical testing (strain rate and loading direction), 4–5 experiments mode during mechanical testing (strain rate and loading direction), 4–5 experiments were carried out, were carried out,results the the results of which of which were were then then averaged. averaged. All the experiments All the experiments were were carried outcarried out in conditions in laboratory laboratory conditions at at room temperature room temperature and 50% airand 50% air humidity. humidity. 3. 3. Experimental Results Using abovemethods, Using the above methods,the thedynamic dynamic tests tests of pine of pine andand lime-tree lime-tree werewere carried carried out. Asout.a result, As a result, their dynamic stress–strain curves, the ultimate strength and deformative characteristics of the their dynamic stress–strain curves, the ultimate strength and deformative characteristics of the specimens specimens cut cutalong alongand andtransverse transverse toto thethe grain were grain wereobtained. Dynamic obtained. Dynamic strain diagrams strain diagramsfor pine and for pine lime-tree underunder and lime-tree uniaxial stress stress uniaxial state are presented state in Figures are presented 2 and 3. 2The in Figures and figures 3. Theshow the averaged figures show the stress–strain curves and appropriate strain rate-strain curves. The spread of the obtained averaged stress–strain curves and appropriate strain rate-strain curves. The spread of the obtained properties was no more properties than was no6%. moreIn than all figures 6%. Insolid lines show all figures solidthe dependences lines of the true stress show the dependences of the of the truespecimen stress of
Materials 2020, 13, 5261 4 of 12 Materials 2020, 13, 5261 4 of 12 Materials 2020, 13, 5261 4 of 12 the specimen on its deformation σ~ε, and the dotted lines (in the lower part of the diagrams) on its deformation σ~ε, and the dotted lines (in the lower part of the diagrams) correspond to the the specimen correspond to on the its deformation history σ~ε,rate of the strain andchange the dotted lines έ~ε (the (in the lower appropriate axis ispart of right). on the the diagrams) history of the strain rate change έ~ε (the appropriate axis is on the right). correspond to the history of the strain rate change έ~ε (the appropriate axis is on the right). Figure 2. Deformation diagrams of pine under loading along and across the grain. Figure Figure 2. Deformation diagrams 2. Deformation diagrams of of pine pine under under loading loading along along and and across across the the grain. grain. Figure 3. Deformation diagrams of lime-tree under loading along and across the grain. Figure 3. Deformation diagrams of lime-tree under loading along and across the grain. Figure Two test 3. Deformation modes diagrams on strain rate of lime-tree were chosen: with under loading along non-destructive andand across the results. destructive grain. From the Twostress–strain obtained test modes on strain rate diagrams, were chosen: it follows that forwith bothnon-destructive wood species the andspecimens destructive cutresults. and loadedFrom the Two test obtained modes on stress–strain strain rate diagrams, were it chosen: follows with that non-destructive for both wood and species along the grain have the largest modulus of the load branch in the diagram, as well as ultimate stress destructive the specimensresults.cutFrom and the obtained loaded and along energy stress–strain diagrams, it follows that for both wood species the grain have the largest modulus of the load branch in the diagram, as well as ultimate absorption. the specimens cut and loaded stress along and the energy Wood endurance grain have absorption. can be theindicated largest modulusin Figure of the load branch 4, where diagramsin the ofdiagram, fivefold as well asofultimate loading a pine stress and energy absorption. specimen with its minor damages (curves 1–5) and a single independent loading of anotherofsimilar Wood endurance can be indicated in Figure 4, where diagrams of fivefold loading a pine Wood specimenwith specimen endurance withitsitscomplete can be minor damages indicated (curves failure (curve in Figure 1–5) 6) are 4, where and a single presented. diagrams independent The diagrams of fivefold loadingon are located loading oftheanother of a pine similar deformation specimen specimen axis with withitsits conditionally minor in order damages complete (curves failure to make (curve it easier 1–5) 6)andareathe to assess single effectindependent presented. loadingare The diagrams of multiple loading of the on another located similar on the steepness of specimen deformation the with load sections its complete axisofconditionally failure the stress–strain in order (curve curves.toThe 6) make are presented. it easier average The to assess strain diagrams rate at the effectloads repeated are located of multiple loadingsthe was ~600–800 on on, −1 deformation the steepnessaxisof the conditionally load sections inoforder to make it easier the stress–strain curves. to The assess the effect average ofrate strain multiple loading at repeated on loads the wassteepness ~600–800of s−1the load , and sections in the case ofofspecimen the stress–strain failure, curves. the strain The average rate strain was about rates−1 2200 at. One repeated loads can clearly was ~600–800 s−1, and in the case of specimen failure, the strain rate was about 2200 s−1. One can clearly
Materials 2020, 13, 5261 5 of 12 Materials 2020, 13, 5261 5 of 12 Materials 2020, 13, 5261 5 of 12 see a decrease in the steepness of the load section of stress–strain curve during repeated loads by a and in the case of specimen failure, the strain rate was about 2200 s−1 . One can clearly see a decrease factor see of 2–3, which a decrease in the is associated steepness withload of the partial destruction section of the specimen of stress–strain during curve during each loading repeated and loads by a in the steepness of the load section of stress–strain curve during repeated loads by a factor of 2–3, violation factor of the of 2–3, flatness which of its ends. is associated with partial destruction of the specimen during each loading and which is associated with partial destruction of the specimen during each loading and violation of the violation of the flatness of its ends. flatness of its ends. Figure 4. An example of multiply repeated loading of the specimen with its minor damage. Figure 4. An example of multiply repeated loading of the specimen with its minor damage. Figure 4. An example of multiply repeated loading of the specimen with its minor damage. As an As animportant importantcharacteristic characteristicof of thethe timber timber damping damping capacity, capacity, the energy the energy absorption absorption of the of the tested tested wood wood Asspeciesspecies an important was estimated characteristic was estimated under of the loading under loading timber along damping along and andcapacity, transverse transverse to thethe toenergy grain the bygrain by calculating absorption calculating ofarea the the the area tested under wood the curve species was σ~ε (Figure estimated under the curve σ~ε (Figure 5). 5). under loading along and transverse to the grain by calculating the area under the curve σ~ε (Figure 5). a) b) a) b) Figure Figure 5. Energy absorption 5. Energy absorption of of the the tested tested wood wood species: species: (a) (a) for for pine, pine, (b) (b) for for lime-tree. lime-tree. Figure 5. Energy absorption of the tested wood species: (a) for pine, (b) for lime-tree. For both wood species, there is a significant excess of energy absorption by the specimens cut and For both wood species, there is a significant excess of energy absorption by the specimens cut tested along the grain, compared to the specimens cut and tested transverse to the grain. and tested For both along woodthespecies, grain, compared there is ato the specimens significant excesscutof and energy tested transverse absorption bytothethespecimens grain. cut It is interesting to compare the results on the damping ability of wood-based materials obtained It is interesting and tested along the to compare grain, comparedthe results to theon the damping specimens ability cut and testedof wood-based transverse tomaterials the grain.obtained by other researchers. In the work [12] the damping capacity of two types of deciduous and coniferous by other researchers.toIncompare It is interesting the workthe [12] the damping results capacity ability on the damping of two of types of deciduous wood-based and coniferous materials obtained wood: beech and spruce under loading in the longitudinal, tangential and radial directions were wood: by otherbeech and spruce researchers. In theunder work [12]loading in the longitudinal, the damping capacity of two tangential types ofand radial directions deciduous were and coniferous compared. The highest specific energy absorbed was noted for specimens under longitudinal loading, compared. wood: beechTheandhighest spruce specific energyinabsorbed under loading was noted the longitudinal, for specimens tangential under and radial longitudinal directions were and the smallest—under tangential loading. This is traditional tendency for wood materials. loading, andThe compared. the highest smallest—under specific tangential energy absorbedloading.was This noted is traditional tendencyunder for specimens for wood materials. longitudinal While While in [14], the damping ability of the mesocarp layer in durian shell (tropical fruit) fruit) was loading, andinthe[14], the damping tangential smallest—under ability of loading. the mesocarp This islayer in durian traditional shell for tendency (tropical wood materials.was investigated investigated and, as aa result of of the research, it was found the the inverse inverse effect: effect: specific specific energy energy absorption While inand, [14],asthe result damping theability research,of itthe was found mesocarp layer in durian shell (tropical absorption fruit) was of the mesocarp investigated and,layer underoflateral as a result loadingitis the research, higher was found than the that inverseunder axial effect: one. This specific energymayabsorption be due to of the mesocarp layer under lateral loading is higher than that under axial one. This may be due to
Materials 2020, 13, 5261 6 of 12 of the mesocarp layer under lateral loading is higher than that under axial one. This may be due to the fact that the durian shell does not have the same clearly pronounced fiber structure as in wood, therefore the authors’ accentuation on the lower strength and damping ability of the material in the axial direction of load application compared to lateral loading refers to the radial and tangential strength of shell of this fruit. 4. Identification and Verification of the Wood Model To describe the behavior of wood under dynamic loads in the library of the LS-DYNA calculation complex, there is model No. 143 MAT_WOOD. This is a model of a transversely isotropic material for solid elements. It is possible to set material properties or use a predefined set of constants, but only for two species of pine growing in the USA: southern yellow pine and Douglas fir. The primary features of the model are: • Transverse isotropy for the elastic constitutive equations (different properties are modeled parallel and perpendicular to the grain). • Yielding with associated plastic flow formulated with separate yield (failure) surfaces for the parallel- and perpendicular-to-the-grain modes. • Hardening in compression formulated with translating yield surfaces. • Post-peak softening formulated with separate damage models for the parallel and perpendicular-to-the-grain modes. • Strength enhancement at high strain rates. Model 143 for pine contains a predefined set of 29 parameters depending on moisture content and temperature. According to the results of the pine tests, some parameters of this model were adjusted for a particular batch of samples under study. These parameters are shown in Table 2. Table 2. Main mechanical properties of pine for model identification. Designation Value Density 450 kg/m3 Modulus of elasticity in the direction of the grain 10,500 MPa Flow stress during compression in the direction of the grain 80 MPa The modulus of elasticity in the direction perpendicular to the grain 246 MPa Flow stress during compression in the direction perpendicular to the grain 10 MPa It should be noted that the elastic moduli of pine under loading along and across the grain were obtained as a result of quasi-static tests, since the Kolsky method, in principle, does not allow constructing a stress–strain curve in which the slope dσ/dε of the elastic loading section would be equal to the static modulus of elasticity. Usually the steepness of this section is several times less than the static Young’s modulus. The reasons for this are as follows: - The difference in the cross-sectional areas of the measuring bars and the sample (some part of the incident wave is reflected from the free surface around the sample), causing an apparent deformation of the sample, - The presence of gaps between the ends of the measuring bars and the sample (due to the non-parallelism of its ends and their roughness or insufficient “pressing” of the sample during the preparation of the test), - Dispersion during the propagation of waves in the bars (decrease in the steepness of the transmitted pulse during the propagation time to the recording strain gauge). In order to confirm the adequacy of the model parameters determined from experiments, it is necessary to verify it, but in experiments other than those in which these parameters were
Materials 2020, 13, 5261 7 of 12 obtained. For Materials 2020, 13,this 5261purpose, we used a model experiment in full-scale and numerical implementation. 7 of 12 The simulation of the indentation process was performed using the finite element method. The explicit Materials performed time 2020, integration 13, 5261 using the schemeDynamics-2 was used for solving the equations of motion in time. Modeling 7was ® software package [20]. The numerical experiment was simulated of 12 in an axisymmetric formulation, performed using the Dynamics-2 software ®and its design corresponded to a similar natural test. package [20]. The numerical experiment was simulated in performed To verify usingthe the Dynamics-2 model of and ® software package [20]. The numerical experiment was simulated material behavior, we usedtoan experimental scheme for dynamic an axisymmetric formulation, its design corresponded a similar natural test. in an axisymmetric indentation by using formulation, the system ofanda its design split corresponded Hopkinson bar. The to a similarprocedure indicated natural test.is schematically To verify the model of material behavior, we used an experimental scheme for dynamic indentation shown To verify the model of material behavior, we used an experimental scheme forhead dynamic by usinginthe Figure system 6. ofThe sample a split 5 and abar. Hopkinson removable indenter The indicated 4 with ais hemispherical procedure schematically shown are in indentation sandwiched by using between the the system measuring of a barssplit 2 Hopkinson and 6. Upon bar. impact The indicated loading by procedure the striker 1,is a schematically compression Figure 6. The sample 5 and a removable indenter 4 with a hemispherical head are sandwiched between shown is impulse ingenerated Figure 6. inThe sample 5 duration and a removable indenteron 4 the with a hemispherical head are the measuring bars 2 andthe bar 2 the 6. Upon impact loadingof which depends by the striker length 1, a compression of the striker impulse and the is generated sandwiched amplitude between theofmeasuring bars 2 and 6. Upon impact loading by the the striker 1, a compression in the bar 2on thethe speed duration the striker. of which depends In the case on the of hemispherical length of the strikerindenter, contact and the amplitude onarea at the the speed impulse initial is moment generated of in the indentation baris 2 the very duration small, of which therefore, thedepends amplitudeon the of length the of the reflected striker pulse and is verythe of the striker. In the case of hemispherical indenter, the contact area at the initial moment of indentation amplitude and significant, on theso speed of theisstriker. the sample loaded In the case of hemispherical indenter, oftheadditional contact area at the is very small, therefore, the amplitude of several times. the reflected For reliable pulse recording is very significant, and so the sample loading is initial cycles, itmoment is necessaryof indentation to increase is very small, therefore, the lengthofofadditional the the supporting amplitude bar of the in comparison reflected pulse withtothe lengthvery is of loaded several times. For reliable recording loading cycles, it is necessary increase the significant, the loading andasso the sample is loaded several times.cycles For reliable recording of additional loading length of thebar much supporting as barrequired to register in comparison withloading the length [21].loading of the bar as much as required to cycles, it is necessary to increase the length of the supporting bar in comparison with the length of register loading cycles [21]. the loading bar as much as required to register loading cycles [21]. Figure 6. High speed indentation experiment scheme. Figure 6. High speed indentation experiment scheme. Using strain gauges 3,Figure elastic6. strain High speed pulses indentation are recordedexperiment in thescheme. measuring bars (Figure 7). The Usingpulses following strainaregauges indicated3, elastic strain 1—incident by numbers: pulses are recorded in thepulse (loading) strain measuring bars (Figure εI(t), 2—reflected pulse7). Using strain gauges R3, elasticby strain pulses1—incident are recorded in theI measuring bars (Figure I (t), 7). The in the first loading cycle ε1 (t ) , 3—incident (loading) strain pulse ε 2 (t ) in the second The following pulses are indicated numbers: (loading) strain pulse ε 2—reflected loading cycle, following pulse in thepulses are indicated first loading cycle εby R (numbers: t), 3—incident1—incident (loading) (loading) strain strain pulse pulse εI(t), εI2 (t) in the2—reflected second loading pulse R T 4—reflected cycle, strain in the4—reflected pulse first loading strain in the cycle pulse R 1 second loading ε1 (t ) ,in3—incident cycle the second(loading) ε 2 loading strain(t ) , 5—transmitted cycle εpulseR I pulse (first ε 2 (t ) in the second (t), 5—transmitted cycle) pulseloading ε 1 (t ) (first cycle) cycle, T 2 T ε, 14—reflected 6—transmitted (t), 6—transmittedpulsepulse (second strain pulse ε 2loading cycle)cycle) in(second the second (tε)2.(t). cycle ε R (t ) , 5—transmitted pulse (first cycle) ε T (t ) T 2 1 T , 6—transmitted pulse (second cycle) ε (t ) . 2 Figure 7. Typical waveform obtained in the experiment for high-speed indentation, taking into account Figure 7. Typical waveform obtained in the experiment for high-speed indentation, taking into additional cycles: upper beam—data from bar 2; lower beam—data from bar 6. account additional cycles: upper beam—data from bar 2; lower beam—data from bar 6. Figure 7. Typical waveform obtained in the experiment for high-speed indentation, taking into The loading of the SHPB system in the numerical experiment (Figure 8) is performed in the same account The additional loading cycles: system of the SHPB upper beam—data from bar in the numerical 2; lower beam—data experiment (Figure 8)from bar 6. is performed in the same way as in the natural experiment—with the help of a striker having an initial velocity V 0 . In the way as in the natural experiment—with the help of a striker having an initial velocity V0. In the The loading calculation ofthe process, theincident SHPB system in the numerical and reflected experiment strain pulses (Figurein8)element are calculated is performed 2 and in thethe same past— way as in the natural experiment—with the help of a striker having an initial in element 6. The time dependences obtained during the simulation are compared with the velocity V 0. In the calculation process, corresponding valuesthe incidentduring recorded and reflected strain pulses are calculated in element 2 and the past— the experiment. in element 6. The time dependences obtained during the simulation are compared with the corresponding values recorded during the experiment.
Materials 2020, 13, 5261 8 of 12 Materials 2020, 13, 5261 8 of 12 calculation process, the incident and reflected strain pulses are calculated in element 2 and the past—in element 6. The time dependences obtained during the simulation are compared with the corresponding Figure 8. High speed indentation experiment simulation scheme. Materialsrecorded values 2020, 13, 5261 during the experiment. 8 of 12 The indenter is made of high-strength tungsten–cobalt alloy and is modeled by a rigid non- deformable material. To assess the processes occurring in the sample, data obtained from measuring bars is used. In accordance with the Kolsky formulas, one can calculate the law of change of the indenter penetration rate into the sample V(t) and the penetration resistance force F(t): Figure 8. High speed V(t) =indentation C1·(εI(t) + εexperiment R(t)) − C2·εsimulation T(t) scheme. Figure 8. High speed indentation experiment simulation scheme. (1) The indenter is made of high-strength F(t) =tungsten–cobalt E2∙S2 εT(t). alloy and is modeled by a rigid The indenter non-deformable is made of high-strength tungsten–cobalt alloy and is modeled by a rigid non- material. here εI(t), εR(t) deformable and εT(t) denote the incident, reflected, and transmitted strain pulses in the measuring material. To assess the processes occurring in the sample, data obtained from measuring bars is used. bars, respectively, To assesswith the Ethe is the elastic processes modulus,the and C is thedata bar obtained velocity of sound. The subscripts 1 and In 2 In accordance Kolskyoccurring formulas, in one can sample, calculate the law of change from measuring of the indenter barspenetration is used. refer to accordance the first (loading) and second (supporting) measuring bars. rate into the with sample theV(t) Kolskyandformulas, the penetrationone can calculateforce resistance the lawF(t):of change of the indenter penetration rate When into the modeling sample V(t) the and process of dynamic resistance the penetration indentation intoF(t): force wood samples, the following scheme was used: a sample and an indenter V(t) = were C1C·(εconsidered I (t) + εR (t))(Figure − C 2·ε 9). The spatial discretization of the ·εTT(t) (t) 1·(εI(t) + εR(t)) − C2 indenter and the sample was doneV(t) by=using a solid F(t) = E2 ·S2 ε (t). T three-dimensional finite element with one (1) (1) integration point. Due to the presence of symmetry, F(t) = E2∙S a 2quarter ε (t). of the geometric model was considered. T On here the I planesR of symmetry, T the corresponding boundary conditions were pulses specified:the at the nodes hereεεI(t), (t), εεR(t) and εεT(t) (t) and (t) denote denote thethe incident, incident, reflected, reflected, and and transmitted transmitted strain strain pulses in in the measuring measuring lying on the plane with the normal in the direction of the oY axis, zero velocities in the oY direction2 bars, respectively,EEisisthe bars,respectively, theelastic elasticmodulus, modulus,and andCCisisthe thebar barvelocity velocityof ofsound. sound.The Thesubscripts subscripts11and and 2 and refer zerothe velocities of rotation about the oX and oZ axes were set; at the nodes lying on the plane with referto to thefirst first(loading) (loading)and andsecond second(supporting) (supporting)measuringmeasuringbars. bars. the normal When in the direction of the oZ axis, zero velocitiesintoin the oZ direction the and zero velocities of Whenmodeling modelingthe theprocess process ofof dynamic dynamic indentation indentation wood into wood samples, samples, following the followingscheme was scheme rotation used: about a sample the oX and anandand oY indenter axes were set. were considered (Figure (Figure 9). The spatial was used: a sample an indenter were considered 9). Thediscretization of the indenter spatial discretization of the and Zero the velocities sample was in theby done direction using a of thethree-dimensional solid oX axis were set at the element finite nodes belonging with one to the surface integration of point. indenter and the sample was done by using a solid three-dimensional finite element with one the Due sample, which to the presence in full-scale of symmetry, experiments a quarter rested against of the geometric the transmitted measuring bar. integration point. Due to the presence of symmetry, a quartermodelof thewas considered. geometric modelOn wasthe planes of considered. The indenter symmetry, was modeledboundary by an absolutely rigid undeformable body. For thelying indenter, the law On the planes of symmetry, the corresponding boundary conditions were specified: at the plane the corresponding conditions were specified: at the nodes on the nodes of thethe with change normal ininthethespeed of itsofmovement direction the oY axis, inzerothe velocities axial direction in the was oY set. The and direction timezerodependence velocities of of lying on the plane with the normal in the direction of the oY axis, zero velocities in the oY direction indenter’s rotation axial about velocity the oX and foroZa particular axes were experiment set; at the was nodes calculated lying on using the the plane Equation with the (1) normal based in on the and zero velocities of rotation about the oX and oZ axes were set; at the nodes lying on the plane with the signals direction ofrecorded the in the oZ axis, zero measuring velocities bars. the normal in the direction of the oZ in thezero axis, oZ direction velocitiesand zerooZ in the velocities direction of and rotation zeroabout the oX velocities of and The oY “surface–surface” axes were set. contact interaction was set between the indenter and the sample. rotation about the oX and oY axes were set. Zero velocities in the direction of the oX axis were set at the nodes belonging to the surface of the sample, which in full-scale experiments rested against the transmitted measuring bar. The indenter was modeled by an absolutely rigid undeformable body. For the indenter, the law of the change in the speed of its movement in the axial direction was set. The time dependence of indenter’s axial velocity for a particular experiment was calculated using the Equation (1) based on the signals recorded in the measuring bars. The “surface–surface” contact interaction was set between the indenter and the sample. a) b) Figure 9.9.Geometric statement Geometric of the statement of problem of numerical the problem simulation: of numerical (a) 3D configuration, simulation: (b) plane (a) 3D configuration, configuration. (b) plane configuration. Zero velocities in the direction of the oX axis were set at the nodes belonging to the surface of the sample, which in full-scale experiments rested against the transmitted measuring bar. The indenter was modeled by an absolutely rigid undeformable body. For the indenter, the law of a) the change in the speed of its movement in the axial b)direction was set. The time dependence of Figure 9. Geometric statement of the problem of numerical simulation: (a) 3D configuration, (b) plane configuration.
Materials 2020, 13, 5261 9 of 12 indenter’s axial velocity for a particular experiment was calculated using the Equation (1) based on the signals recorded in the measuring bars. Materials 2020, 13, 5261 9 of 12 The “surface–surface” contact interaction was set between the indenter and the sample. InInnatural naturalexperiments experiments on on the the indentation thesamples indentation the samplesofofpinepinewere wereused used ininthethe form form of of tablets tablets with with a length of 10 mm and a diameter of 20 mm. Some of the samples were cut in the directionof a length of 10 mm and a diameter of 20 mm. Some of the samples were cut in the direction ofthe wood grain,grain, the wood whilewhile another partpart another of the samples of the waswas samples cutcut in in thethe perpendicular perpendiculartotothethegrain graindirection. direction. AsAs mentioned mentionedabove,above,ininthe the process process of dynamic dynamicindentation, indentation,the thesample sample is is subjected subjected to to multiple multiple loading loading ininthe theexperiment experiment(see(seeFigure Figure 7), thus thusundergoing undergoingaacertain certaindeformation deformation in in each each loading loading cycle. cycle. High-speed High-speed filmfilm recording recording of the of the indentation indentation process process makes makes it possible it possible to estimate to estimate a number a number of of loading loading cycle and cycle and indentation indentation depth atdepth which at which the destruction the destruction of theofmaterial the material occurs. occurs. Figure Figure 1010shows showsthe the frames frames of such of such registration, registration, made made usingusing a high-speed a high-speed camera camera HSFCHSFC Pro. Pro. Figure 10. High-speed Figure10. registrationofofdynamic High-speed registration dynamicindentation. indentation. TheThe left part left of of part thethe figure corresponds figure corresponds to the experiment to the experiment with thethe with sample cutcut sample in the direction in the along direction thealong grain, whereas the right part corresponds to the experiment with the the grain, whereas the right part corresponds to the experiment with the sample cut in the sample cut in the direction transverse direction to the grain. transverse to The numbers the grain. Theon the left on numbers of the the high-speed registration left of the high-speed images indicate registration imagesthe number indicate ofthe loading number cycles (running of loading number cycles of impulse (running numberinof the loadinginmeasuring impulse the loadingbar) which one measuring bar)can seewhich in Figure 7. It can be seen in Figure 10 that the samples cutting off parallel to one can see in Figure 7. It can be seen in Figure 10 that the samples cutting off parallel to thethe grain remain intact throughout grain remain theintact experiment, throughout whichtheisexperiment, confirmed by the final which state of such is confirmed by thesamples. Samples final state of such obtained samples. by cutting Samples in the direction obtained perpendicular by cutting to the grain in the direction retain their perpendicular integrity to the duringtheir grain retain the integrity first loading cycle, during however, the first cracks loadingand cycle,gaps between however, the layers cracks and gapsof wood between appear in theofsecond the layers cycle, which wood appear in the grow secondand cycle, which progress grow and loading in subsequent progresscycles, in subsequent leadingloading cycles, leading to the separation of theto sample the separation of the sample into parts. intoIt parts. can be noted that for the same load amplitude, the samples obtained by cutting in the direction It canremain of the fiber be noted that for intact, thethe while same load amplitude, samples the samples cut perpendicular obtained to the by cutting fiber exhibit in the failure direction already in the of the fiber first loading cycle.remain intact, while the samples cut perpendicular to the fiber exhibit failure already in the first loading cycle. A comparison of the shape of the imprint on the pine sample after the experiment on the dynamic indentation of a hemispherical indenter is shown in Figure 11.
Materials 2020, 13, 5261 10 of 12 A comparison of the shape of the imprint on the pine sample after the experiment on the dynamic indentation Materials 2020, Materials of 5261 2020, 13, 13, a hemispherical indenter is shown in Figure 11. 5261 10 of 10 of 12 12 a) b) Figure 11. Figure11. Figure The shape Theshape 11.The ofofthe shapeof the imprints theimprints obtained imprintsobtained by obtainedby numerical bynumerical modeling numericalmodeling (a) modeling(a) and (a)and in andin the inthe natural thenatural test naturaltest (b). test(b). (b). Figure 12 shows Figure shows a comparison comparison of the time dependences dependences of the indentation resistance resistance of pine sample recorded in the experiments (solid colored lines) with the data obtained by numerical sample recorded in the experiments (solid colored lines) with the data obtained by numerical modeling (black dashed lines) during dynamic indentation of hemispherical indenter into specimen both modeling (black dashed lines) during dynamic indentation of hemispherical indenter into specimen along and across both along the andgrain. across the grain. Figure 12. Figure Comparison of 12. Comparison of experimental experimental and and calculated calculated pulses pulses in in the the supporting supporting bar. bar. Figure 12. Comparison of experimental and calculated pulses in the supporting bar. It can be seen that the model used allows us to accurately reproduce the features of the deformation It can be seen that the model used allows us to accurately reproduce the features of the of real material, namely, the difference in its deformation behavior in different directions with respect deformation of real material, namely, the difference in its deformation behavior in different directions to grain orientation. with respect to grain orientation. The results obtained are in qualitative agreement with the data from previous studies of high The results obtained are in qualitative agreement with the data from previous studies of high strain rate behavior of wood [8,17]. Correction of some parameters of the MAT_WOOD model made it strain rate behavior of wood [8,17]. Correction of some parameters of the MAT_WOOD model made it possibletotodescribe possible describethe thedeformation deformationbehavior behaviorof of the the studied studied wood species with wood species with sufficient sufficientaccuracy. accuracy. A further increase in the quality of the mathematical model is possible by taking into account the effect A further increase in the quality of the mathematical model is possible by taking into account the of the of effect strain rate inrate the strain a wide in arange wideof its change, range as well as of its change, as well taking asinto account taking the fracture into account of the material. the fracture of the material. In addition, it is necessary to conduct more complex model experiments to verify the fracture criteria, for example, high-speed penetration and perforation of wood plates.
Materials 2020, 13, 5261 11 of 12 In addition, it is necessary to conduct more complex model experiments to verify the fracture criteria, for example, high-speed penetration and perforation of wood plates. 5. Conclusions Dynamic tests of lime-tree and pine were conducted. There is a strong anisotropy of the properties of the tested materials: the specimens exhibit the greatest strength under load applied along the grain, while the lowest strength is observed under loading transverse to the grain. The load branch module is non-linear and, as a rule, smaller than the unloading branch module (while maintaining the specimen integrity). At the specimen cutting angle of 90◦ with respect to the direction of the fibers, the stress–strain diagram after reaching a certain threshold stress value (about 8 MPa for lime-tree and about 10 MPa for pine) is close to the ideal plastic diagram. At 0◦ cutting angle, the initial section of the diagrams is close to linear. That is, an elastic deformation occurs. However, after reaching an ultimate stress value (yield strength), the diagram becomes nonlinear with stress relaxation. Especially such behavior is observed in the experiments in which the failure of specimens occurs. Using a modification of the SHPB method, experiments were performed on the dynamic indentation of indenters with a hemispherical head into the samples parallel and perpendicular to the direction of the fibers. Dependences of resistance to penetration on time are constructed. In the direction of the fiber (along the grain), the resistance force was more than three-times greater than in the transverse direction. The results of the natural experiment were compared with the results of numerical modeling, in which the wood behavior was described by the MAT_WOOD model from the LS-DYNA software, in which some of the parameters were obtained experimentally. A good coincidence was observed. Author Contributions: Conceptualization, A.B. and L.I.; data curation, T.I.; formal analysis, A.K.; funding acquisition, L.I.; investigation, A.L.; methodology, A.K. and A.L.; project administration, A.B.; resources, L.I.; software, A.K. and T.I.; supervision, F.d.; validation, F.d. and A.K.; visualization, A.K.; writing—original draft, A.L.; writing—review and editing, A.B. All authors have read and agreed to the published version of the manuscript. Funding: Experimental investigations of wood were performed with the financial support of the Ministry of Science and Higher Education of the Russian Federation (task 0729-2020-0054). Numerical simulation of wood behavior was supported by the grant of the Government of the Russian Federation (contract No.14.Y26.31.0031). Conflicts of Interest: The authors declare no conflict of interest. The funders had no role in the design of the study; in the collection, analyses, or interpretation of data; in the writing of the manuscript, or in the decision to publish the results. References 1. Murray, Y.D. Manual for LS-DYNA Wood Material Model 143; Publication No. FHWA-HRT-04-097; Federal Highway Administration: Washington, DC, USA, 2007. 2. Johnson, W. Historical and present-day references concerning impact on wood. Int. J. Impact Eng. 1986, 4, 161–174. [CrossRef] 3. Neumann, M. Investigation of the Behavior of Shock-Absorbing Structural Parts of Transport Casks Holding Radioactive Substances in Terms of Design Testing and Risk Analysis. Ph.D. Thesis, Bergische Universität Wuppertal, Wuppertal, Germany, 2009. 4. Reid, S.R.; Reddy, T.Y.; Peng, C. Dynamic compression of cellular structures and materials. In Structural Crashworthiness and Failure; Jones, N., Wierzbicki, T., Eds.; Taylor & Francis Publication: London, UK; New York, NY, USA, 1993; pp. 257–294. 5. Reid, S.R.; Peng, C. Dynamic Uniaxial Crushing of Wood. Int. J. Impact Eng. 1997, 19, 531–570. [CrossRef] 6. Harrigan, J.J.; Reid, S.R.; Tan, P.J.; Reddy, T.Y. High rate crushing of wood along the grain. Int. J. Mech. Sci. 2005, 47, 521–544. [CrossRef] 7. Mania, P.; Siuda, F.; Roszyk, E. Effect of Slope Grain on Mechanical Properties of Different Wood Species. Materials 2020, 13, 1503. [CrossRef] [PubMed] 8. Bragov, A.M.; Lomunov, A.K. Dynamic properties of some wood species. J. Phys. IV 1997, 7, 487–492. [CrossRef]
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